Technology Process of C19H16BFN2O4
There total 6 articles about C19H16BFN2O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C25H26BFN2O4;
With
potassium hydrogen difluoride;
In
methanol; water;
at 20 ℃;
With
chloro-trimethyl-silane;
In
water; acetonitrile;
for 1h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline / N,N-dimethyl-formamide / 20 °C
2.1: potassium tert-butylate; 18-crown-6 ether / 1,4-dioxane / 2 h / Reflux
3.1: potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2 / 1-methyl-pyrrolidin-2-one / 16 h / 80 °C / Inert atmosphere
4.1: potassium hydrogen difluoride / water; methanol / 20 °C
4.2: 1 h
With
potassium hydrogen difluoride; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; 18-crown-6 ether; potassium acetate; potassium tert-butylate; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline;
In
1,4-dioxane; 1-methyl-pyrrolidin-2-one; methanol; water; N,N-dimethyl-formamide;