N-benzyloxycarbonyl-O-(2,3,5,6-tetra-O-acetyl-β-D-galactofuranosyl)-L-serinyl methyl ester

Base Information

Chemical Name:N-benzyloxycarbonyl-O-(2,3,5,6-tetra-O-acetyl-β-D-galactofuranosyl)-L-serinyl methyl ester
CAS No.:4671-52-7
Molecular Formula:C₂₆H₃₃NO₁₄
Molecular Weight:583.546
Hs Code.:

Synonyms:N-benzyloxycarbonyl-O-(2,3,5,6-tetra-O-acetyl-β-D-galactofuranosyl)-L-serinyl methyl ester

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Chemical Property of N-benzyloxycarbonyl-O-(2,3,5,6-tetra-O-acetyl-β-D-galactofuranosyl)-L-serinyl methyl ester

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Technology Process of N-benzyloxycarbonyl-O-(2,3,5,6-tetra-O-acetyl-β-D-galactofuranosyl)-L-serinyl methyl ester

There total 5 articles about N-benzyloxycarbonyl-O-(2,3,5,6-tetra-O-acetyl-β-D-galactofuranosyl)-L-serinyl methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 396716-71-5
2,3,5,6-tetra-O-acetyl-β-D-galactofuranosyl trichloroacetimidate

: 1676-81-9
N-benzyloxycarbonyl-L-serine methyl ester

: 4671-52-7
N-benzyloxycarbonyl-O-(2,3,5,6-tetra-O-acetyl-β-D-galactofuranosyl)-L-serinyl methyl ester

Guidance literature:: 2,3,5,6-tetra-O-acetyl-β-D-galactofuranosyl trichloroacetimidate; N-benzyloxycarbonyl-L-serine methyl ester; With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 1h; Molecular sieve;

Molecular sieve; Inert atmosphere;
DOI:10.1016/j.tetlet.2011.01.001

Reference yield: 65.0%

: 1676-81-9
N-benzyloxycarbonyl-L-serine methyl ester

: 5531-53-3,10535-09-8,22435-12-7,40031-23-0,55123-31-4,72002-47-2,72691-27-1,72691-28-2,62181-82-2
1,2,3,5,6-penta-O-acetyl-α,β-D-galactofuranose

: 4671-52-7
N-benzyloxycarbonyl-O-(2,3,5,6-tetra-O-acetyl-β-D-galactofuranosyl)-L-serinyl methyl ester

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 0 ℃; Inert atmosphere;
DOI:10.1016/j.tetlet.2011.01.001

Reference yield: 48.0%

: 1676-81-9
N-benzyloxycarbonyl-L-serine methyl ester

: 4671-52-7
N-benzyloxycarbonyl-O-(2,3,5,6-tetra-O-acetyl-β-D-galactofuranosyl)-L-serinyl methyl ester

Guidance literature:: With copper(II) bis(trifluoromethanesulfonate); In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.tetlet.2011.01.001