anti-methyl 3-(3,4-dimethoxyphenyl)-3-hydroxy-2-(3-methoxyphenyl)propanoate

Base Information

Chemical Name:anti-methyl 3-(3,4-dimethoxyphenyl)-3-hydroxy-2-(3-methoxyphenyl)propanoate
CAS No.:1431563-91-5
Molecular Formula:C₁₉H₂₂O₆
Molecular Weight:346.38
Hs Code.:

Synonyms:anti-methyl 3-(3,4-dimethoxyphenyl)-3-hydroxy-2-(3-methoxyphenyl)propanoate

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Chemical Property of anti-methyl 3-(3,4-dimethoxyphenyl)-3-hydroxy-2-(3-methoxyphenyl)propanoate

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Technology Process of anti-methyl 3-(3,4-dimethoxyphenyl)-3-hydroxy-2-(3-methoxyphenyl)propanoate

There total 3 articles about anti-methyl 3-(3,4-dimethoxyphenyl)-3-hydroxy-2-(3-methoxyphenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1431563-77-7
(2S,3S)-methyl 3-((tert-butyldimethylsilyl)oxy)-3-(3,4-dimethoxyphenyl)-2-(3-methoxyphenyl)propanoate

: 1431563-89-1
(2S,3S)-methyl 3-(3,4-dimethoxyphenyl)-3-hydroxy-2-(3-methoxyphenyl)propanoate

: 1431563-91-5
anti-methyl 3-(3,4-dimethoxyphenyl)-3-hydroxy-2-(3-methoxyphenyl)propanoate

Guidance literature:: With hydrogen fluoride; In acetonitrile; at 23 ℃; Inert atmosphere;
DOI:10.1021/ja401731d

Reference yield:

: 384365-49-5
methyl 2-diazo-2-(3-methoxyphenyl)acetate

: 1431563-89-1
(2S,3S)-methyl 3-(3,4-dimethoxyphenyl)-3-hydroxy-2-(3-methoxyphenyl)propanoate

: 1431563-91-5
anti-methyl 3-(3,4-dimethoxyphenyl)-3-hydroxy-2-(3-methoxyphenyl)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: dirhodium(II) tetrakis[N-phthaloyl-(S)-tert-leucinate] / 50 °C / Inert atmosphere

2: hydrogen fluoride / acetonitrile / 23 °C / Inert atmosphere

With dirhodium(II) tetrakis[N-phthaloyl-(S)-tert-leucinate]; hydrogen fluoride; In acetonitrile;
DOI:10.1021/ja401731d

Reference yield:

: 4-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-1,2-dimethoxybenzene

: 1431563-89-1
(2S,3S)-methyl 3-(3,4-dimethoxyphenyl)-3-hydroxy-2-(3-methoxyphenyl)propanoate

: 1431563-91-5
anti-methyl 3-(3,4-dimethoxyphenyl)-3-hydroxy-2-(3-methoxyphenyl)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: dirhodium(II) tetrakis[N-phthaloyl-(S)-tert-leucinate] / 50 °C / Inert atmosphere

2: hydrogen fluoride / acetonitrile / 23 °C / Inert atmosphere

With dirhodium(II) tetrakis[N-phthaloyl-(S)-tert-leucinate]; hydrogen fluoride; In acetonitrile;
DOI:10.1021/ja401731d