ethyl N-nitroso-N-methyl-bis{9-[10-(4-tert-butyl-2,6-dimethyl)phenyl]anthryl}carbamate

Base Information

Chemical Name:ethyl N-nitroso-N-methyl-bis{9-[10-(4-tert-butyl-2,6-dimethyl)phenyl]anthryl}carbamate
CAS No.:648418-80-8
Molecular Formula:C₅₆H₅₆N₂O₃
Molecular Weight:805.072
Hs Code.:

Synonyms:ethyl N-nitroso-N-methyl-bis{9-[10-(4-tert-butyl-2,6-dimethyl)phenyl]anthryl}carbamate

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Chemical Property of ethyl N-nitroso-N-methyl-bis{9-[10-(4-tert-butyl-2,6-dimethyl)phenyl]anthryl}carbamate

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Technology Process of ethyl N-nitroso-N-methyl-bis{9-[10-(4-tert-butyl-2,6-dimethyl)phenyl]anthryl}carbamate

There total 7 articles about ethyl N-nitroso-N-methyl-bis{9-[10-(4-tert-butyl-2,6-dimethyl)phenyl]anthryl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 648418-79-5
ethyl N-methyl-bis{9-[10-(4-tert-butyl-2,6-dimethyl)phenyl]anthryl}carbamate

: 648418-80-8
ethyl N-nitroso-N-methyl-bis{9-[10-(4-tert-butyl-2,6-dimethyl)phenyl]anthryl}carbamate

Guidance literature:: With sodium acetate; dinitrogen tetraoxide; In tetrachloromethane; at 20 ℃; for 2h;
DOI:10.1021/ja038423z

Reference yield:

: 5345-05-1
4-t-butyl-2,6-dimethylbromobenzene

: 648418-80-8
ethyl N-nitroso-N-methyl-bis{9-[10-(4-tert-butyl-2,6-dimethyl)phenyl]anthryl}carbamate

Guidance literature:: Multi-step reaction with 6 steps

1.1: n-BuLi / diethyl ether; hexane / 20 °C

1.2: 32 percent / toluene; diethyl ether; hexane / Heating

2.1: 82 percent / bromine / CCl₄ / 20 °C

3.1: n-BuLi / diethyl ether; hexane / 2 h / 0 °C

3.2: 79 percent / diethyl ether; hexane / Heating

4.1: HCl(gas) / benzene / 0.5 h / 5 °C

5.1: 589 mg / AgBF₄ / dioxane / Heating

6.1: N₂O₄; sodium acetate / CCl₄ / 2 h / 20 °C

With hydrogenchloride; silver tetrafluoroborate; n-butyllithium; bromine; sodium acetate; dinitrogen tetraoxide; In 1,4-dioxane; tetrachloromethane; diethyl ether; hexane; benzene;
DOI:10.1021/ja038423z

Reference yield:

: 648418-75-1
9-(4-tert-butyl-2,6-dimethylphenyl)anthracene

: 648418-80-8
ethyl N-nitroso-N-methyl-bis{9-[10-(4-tert-butyl-2,6-dimethyl)phenyl]anthryl}carbamate

Guidance literature:: Multi-step reaction with 5 steps

1.1: 82 percent / bromine / CCl₄ / 20 °C

2.1: n-BuLi / diethyl ether; hexane / 2 h / 0 °C

2.2: 79 percent / diethyl ether; hexane / Heating

3.1: HCl(gas) / benzene / 0.5 h / 5 °C

4.1: 589 mg / AgBF₄ / dioxane / Heating

5.1: N₂O₄; sodium acetate / CCl₄ / 2 h / 20 °C

With hydrogenchloride; silver tetrafluoroborate; n-butyllithium; bromine; sodium acetate; dinitrogen tetraoxide; In 1,4-dioxane; tetrachloromethane; diethyl ether; hexane; benzene;
DOI:10.1021/ja038423z