(S)-methyl 3-(4-(benzyloxy)phenyl)-2-(N-((R)-3-(tert-butyldimethylsilyloxy)-2-(2-nitrophenylamino)propyl)-4-methylphenylsulfonamido)propanoate

Base Information

• Chemical Name: (S)-methyl 3-(4-(benzyloxy)phenyl)-2-(N-((R)-3-(tert-butyldimethylsilyloxy)-2-(2-nitrophenylamino)propyl)-4-methylphenylsulfonamido)propanoate
• CAS No.: 1236362-45-0
• Molecular Formula: C₃₉H₄₉N₃O₈SSi
• Molecular Weight: 747.985

Synonyms:(S)-methyl 3-(4-(benzyloxy)phenyl)-2-(N-((R)-3-(tert-butyldimethylsilyloxy)-2-(2-nitrophenylamino)propyl)-4-methylphenylsulfonamido)propanoate

Chemical Property of (S)-methyl 3-(4-(benzyloxy)phenyl)-2-(N-((R)-3-(tert-butyldimethylsilyloxy)-2-(2-nitrophenylamino)propyl)-4-methylphenylsulfonamido)propanoate

Chemical Property:

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Technology Process of (S)-methyl 3-(4-(benzyloxy)phenyl)-2-(N-((R)-3-(tert-butyldimethylsilyloxy)-2-(2-nitrophenylamino)propyl)-4-methylphenylsulfonamido)propanoate

There total 1 articles about (S)-methyl 3-(4-(benzyloxy)phenyl)-2-(N-((R)-3-(tert-butyldimethylsilyloxy)-2-(2-nitrophenylamino)propyl)-4-methylphenylsulfonamido)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

C24H25NO5S (175214-62-7) + (R)-3-(tert-butyldimethylsilyloxy)-2-(2-nitrophenylamino)propan-1-ol (1236362-34-7) → (S)-methyl 3-(4-(benzyloxy)phenyl)-2-(N-((R)-3-(tert-butyldimethylsilyloxy)-2-(2-nitrophenylamino)propyl)-4-methylphenylsulfonamido)propanoate (1236362-45-0)

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 0 - 25 ℃;

DOI:10.1039/c000029a

Reference yield:

(S)-methyl 3-(4-(benzyloxy)phenyl)-2-(N-((R)-3-(tert-butyldimethylsilyloxy)-2-(2-nitrophenylamino)propyl)-4-methylphenylsulfonamido)propanoate (1236362-45-0) → C33H35N3O8S (1236362-53-0)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere;

DOI:10.1039/c000029a

upstream raw materials:

C₂₄H₂₅NO₅S

(R)-3-(tert-butyldimethylsilyloxy)-2-(2-nitrophenylamino)propan-1-ol

Downstream raw materials:

C₃₃H₃₅N₃O₈S

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