(±)-cyclopropyl(imino)(phenyl)-λ⁶-sulfanone

Base Information

• Chemical Name: (±)-cyclopropyl(imino)(phenyl)-λ⁶-sulfanone
• CAS No.: 50337-61-6
• Molecular Formula: C₉H₁₁NOS
• Molecular Weight: 181.258
• Mol file: 50337-61-6.mol

Synonyms:(±)-cyclopropyl(imino)(phenyl)-λ⁶-sulfanone

Chemical Property of (±)-cyclopropyl(imino)(phenyl)-λ⁶-sulfanone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of (±)-cyclopropyl(imino)(phenyl)-λ⁶-sulfanone

There total 5 articles about (±)-cyclopropyl(imino)(phenyl)-λ⁶-sulfanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

N-(2,2,2-trifluoroethyloxycarbonyl)cyclopropyl phenyl sulfoximine → (±)-cyclopropyl(imino)(phenyl)-λ6-sulfanone (50337-61-6)

Guidance literature:

With sulfuric acid; In water; at 110 ℃; for 2h;

DOI:10.1002/adsc.201300766

Reference yield: 91.0%

cyclopropylphenylsulfide (14633-54-6) → (±)-cyclopropyl(imino)(phenyl)-λ6-sulfanone (50337-61-6)

Guidance literature:

With [bis(acetoxy)iodo]benzene; ammonium carbamate; In methanol; at 20 ℃; for 0.5h;

DOI:10.1039/c6cc09940h

Reference yield: 90.0%

cyclopropyl phenyl sulfoxide (50337-59-2) → (±)-cyclopropyl(imino)(phenyl)-λ6-sulfanone (50337-61-6)

Guidance literature:

With sodium azide; In neat (no solvent); at 50 ℃; for 0.5h;

DOI:10.1016/j.tetlet.2016.12.031

upstream raw materials:

cyclopropyl phenyl sulfoxide

cyclopropylphenylsulfide

thiophenol