Azoture de l'acide 2-diethylphosphono-3-phenylpropanoique

Base Information

Chemical Name:Azoture de l'acide 2-diethylphosphono-3-phenylpropanoique
CAS No.:146036-71-7
Molecular Formula:C₁₃H₁₈N₃O₄P
Molecular Weight:311.277
Hs Code.:

Synonyms:Azoture de l'acide 2-diethylphosphono-3-phenylpropanoique

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Chemical Property of Azoture de l'acide 2-diethylphosphono-3-phenylpropanoique

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Technology Process of Azoture de l'acide 2-diethylphosphono-3-phenylpropanoique

There total 2 articles about Azoture de l'acide 2-diethylphosphono-3-phenylpropanoique which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 146036-61-5
(1-Chlorocarbonyl-2-phenyl-ethyl)-phosphonic acid diethyl ester

: 146036-71-7
Azoture de l'acide 2-diethylphosphono-3-phenylpropanoique

Guidance literature:: With sodium azide; In diethyl ether; water; for 2h; < 5 deg C;
DOI:10.1016/S0040-4020(01)92278-1

Reference yield:

: 86963-66-8
2-(diethoxyphosphoryl)-3-phenylpropanoic acid

: 146036-71-7
Azoture de l'acide 2-diethylphosphono-3-phenylpropanoique

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / CH₂Cl₂

2: 100 percent / NaN₃ / H₂O; diethyl ether / 2 h / < 5 deg C

With thionyl chloride; sodium azide; In diethyl ether; dichloromethane; water;
DOI:10.1016/S0040-4020(01)92278-1