Technology Process of C29H31N2O3(1+)*Cl(1-)
There total 5 articles about C29H31N2O3(1+)*Cl(1-) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C31H35N2O3(1+)*Cl(1-);
With
boron tribromide;
In
dichloromethane;
at -78 - 20 ℃;
In
methanol;
at 20 ℃;
DOI:10.1021/jo800902j
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: water / 6 h / 200 °C / Autoclave
2.1: pyridine / dichloromethane / 0.25 h / 0 °C
2.2: 24 h / 0 - 20 °C
3.1: dimethyl sulfoxide / 12 h / 90 °C
4.1: tetrahydrofuran / 12 h / 0 - 20 °C
4.2: 0.17 h
5.1: boron tribromide / dichloromethane / -78 - 20 °C
5.2: Amberlite IRA-400 (CI) ion exchange resin / 1 h / 20 °C
With
pyridine; boron tribromide;
In
tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: dimethyl sulfoxide / 12 h / 90 °C
2.1: tetrahydrofuran / 12 h / 0 - 20 °C
2.2: 0.17 h
3.1: boron tribromide / dichloromethane / -78 - 20 °C
3.2: Amberlite IRA-400 (CI) ion exchange resin / 1 h / 20 °C
With
boron tribromide;
In
tetrahydrofuran; dichloromethane; dimethyl sulfoxide;