Acetic acid (S)-2-methyl-3-((E)-3-p-tolylsulfanyl-allyl)-cyclopent-1-enyl ester

Base Information

Chemical Name:Acetic acid (S)-2-methyl-3-((E)-3-p-tolylsulfanyl-allyl)-cyclopent-1-enyl ester
CAS No.:110366-53-5
Molecular Formula:C₁₈H₂₂O₂S
Molecular Weight:302.437
Hs Code.:

Synonyms:Acetic acid (S)-2-methyl-3-((E)-3-p-tolylsulfanyl-allyl)-cyclopent-1-enyl ester

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Chemical Property of Acetic acid (S)-2-methyl-3-((E)-3-p-tolylsulfanyl-allyl)-cyclopent-1-enyl ester

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Technology Process of Acetic acid (S)-2-methyl-3-((E)-3-p-tolylsulfanyl-allyl)-cyclopent-1-enyl ester

There total 5 articles about Acetic acid (S)-2-methyl-3-((E)-3-p-tolylsulfanyl-allyl)-cyclopent-1-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 110416-47-2
<3(S),S(R)>-1-acetoxy-2-methyl-3-<(E)-3-(p-tolylsulfinyl)-2-propen-1-yl>-1-cyclopentene

: 110366-53-5
Acetic acid (S)-2-methyl-3-((E)-3-p-tolylsulfanyl-allyl)-cyclopent-1-enyl ester

Guidance literature:: With acetic acid; zinc; for 10h; Ambient temperature;
DOI:10.1021/jo00381a002

Reference yield:

: 1120-73-6
2-methyl-2-cyclopenten-1-one

: 110366-53-5
Acetic acid (S)-2-methyl-3-((E)-3-p-tolylsulfanyl-allyl)-cyclopent-1-enyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) lithium diisopropylamide (LDA) / 1.) THF, -78 deg C, 1 h, 2.) THF, -78 deg C, 5 min

2: tetrahydrofuran / -78 °C

3: 95 percent / Zn, acetic acid / 10 h / Ambient temperature

With acetic acid; zinc; lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1021/jo00381a002

Reference yield:

: 89708-79-2
(R)-(+)-allyl p-tolyl sulphoxide

: 110366-53-5
Acetic acid (S)-2-methyl-3-((E)-3-p-tolylsulfanyl-allyl)-cyclopent-1-enyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) lithium diisopropylamide (LDA) / 1.) THF, -78 deg C, 1 h, 2.) THF, -78 deg C, 5 min

2: tetrahydrofuran / -78 °C

3: 95 percent / Zn, acetic acid / 10 h / Ambient temperature

With acetic acid; zinc; lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1021/jo00381a002