diethyl bis(3',5'-dimethylbenzyl)methylmalonate

Base Information

Chemical Name:diethyl bis(3',5'-dimethylbenzyl)methylmalonate
CAS No.:930782-30-2
Molecular Formula:C₂₆H₃₄O₄
Molecular Weight:410.554
Hs Code.:

Synonyms:diethyl bis(3',5'-dimethylbenzyl)methylmalonate

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Chemical Property of diethyl bis(3',5'-dimethylbenzyl)methylmalonate

Chemical Property:

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Technology Process of diethyl bis(3',5'-dimethylbenzyl)methylmalonate

There total 1 articles about diethyl bis(3',5'-dimethylbenzyl)methylmalonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 27129-86-8
1-bromomethyl-3,5-dimethylbenzene

: 87-13-8
diethyl 2-ethoxymethylenemalonate

: 930782-30-2
diethyl bis(3',5'-dimethylbenzyl)methylmalonate

Guidance literature:: With magnesium; In diethyl ether; for 18h; Heating;
DOI:10.1021/ja066018c

Reference yield:

: 930782-30-2
diethyl bis(3',5'-dimethylbenzyl)methylmalonate

: 930782-31-3
bis-(3',5'-dimethylbenzyl)methylmalonic acid

Guidance literature:: With sodium hydroxide; In methanol; for 4h; Heating;
DOI:10.1021/ja066018c

Reference yield:

: 930782-30-2
diethyl bis(3',5'-dimethylbenzyl)methylmalonate

: 2-[1-(3,5-dimethyl-benzyl)-2-(3,5-dimethyl-phenyl)-ethyl]-propanedioyl dichloride

Guidance literature:: Multi-step reaction with 2 steps

1: 3.71 g / aqueous NaOH / methanol / 4 h / Heating

2: phosphorus pentachloride / benzene / 3 h / 20 °C

With sodium hydroxide; phosphorus pentachloride; In methanol; benzene;
DOI:10.1021/ja066018c