N-benzyl-N-benzyloxycarbonyl-O-tert-butyldiphenylsilyl-L-serine methyl ester

Base Information

Chemical Name:N-benzyl-N-benzyloxycarbonyl-O-tert-butyldiphenylsilyl-L-serine methyl ester
CAS No.:158012-76-1
Molecular Formula:C₃₅H₃₉NO₅Si
Molecular Weight:581.784
Hs Code.:

Synonyms:N-benzyl-N-benzyloxycarbonyl-O-tert-butyldiphenylsilyl-L-serine methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-benzyl-N-benzyloxycarbonyl-O-tert-butyldiphenylsilyl-L-serine methyl ester

Chemical Property:

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Technology Process of N-benzyl-N-benzyloxycarbonyl-O-tert-butyldiphenylsilyl-L-serine methyl ester

There total 4 articles about N-benzyl-N-benzyloxycarbonyl-O-tert-butyldiphenylsilyl-L-serine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.4%

: 158012-74-9
N-benzyl-N-benzyloxycarbonyl-L-serine methyl ester

: 58479-61-1
tert-butylchlorodiphenylsilane

: 158012-76-1
N-benzyl-N-benzyloxycarbonyl-O-tert-butyldiphenylsilyl-L-serine methyl ester

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 60 ℃; for 3h;

Reference yield:

: 123639-56-5
(S)-N-benzylserine methyl ester

: 158012-76-1
N-benzyl-N-benzyloxycarbonyl-O-tert-butyldiphenylsilyl-L-serine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 82.7 percent / aq. NaHCO₃ / ethyl acetate / Ambient temperature

2: 58.4 percent / imidazole / dimethylformamide / 3 h / 60 °C

With 1H-imidazole; sodium hydrogencarbonate; In ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 40216-75-9
N-benzylidene-L-serine methyl ester

: 158012-76-1
N-benzyl-N-benzyloxycarbonyl-O-tert-butyldiphenylsilyl-L-serine methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: NaBH₄ / 0 °C

2: 82.7 percent / aq. NaHCO₃ / ethyl acetate / Ambient temperature

3: 58.4 percent / imidazole / dimethylformamide / 3 h / 60 °C

With 1H-imidazole; sodium tetrahydroborate; sodium hydrogencarbonate; In ethyl acetate; N,N-dimethyl-formamide;