bis-(4-bromophenyl)-[4-(1-(1-deuteriobutyl)-3-{2-[(triisopropylsilanyl)ethynyl]cyclohex-1-enyl}propa-1,2-dienyl)phenyl]-amine

Base Information

• Chemical Name: bis-(4-bromophenyl)-[4-(1-(1-deuteriobutyl)-3-{2-[(triisopropylsilanyl)ethynyl]cyclohex-1-enyl}propa-1,2-dienyl)phenyl]-amine
• CAS No.: 1173838-55-5
• Molecular Formula: C₄₂H₅₁Br₂NSi
• Molecular Weight: 758.759

Synonyms:bis-(4-bromophenyl)-[4-(1-(1-deuteriobutyl)-3-{2-[(triisopropylsilanyl)ethynyl]cyclohex-1-enyl}propa-1,2-dienyl)phenyl]-amine

Chemical Property of bis-(4-bromophenyl)-[4-(1-(1-deuteriobutyl)-3-{2-[(triisopropylsilanyl)ethynyl]cyclohex-1-enyl}propa-1,2-dienyl)phenyl]-amine

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Technology Process of bis-(4-bromophenyl)-[4-(1-(1-deuteriobutyl)-3-{2-[(triisopropylsilanyl)ethynyl]cyclohex-1-enyl}propa-1,2-dienyl)phenyl]-amine

There total 1 articles about bis-(4-bromophenyl)-[4-(1-(1-deuteriobutyl)-3-{2-[(triisopropylsilanyl)ethynyl]cyclohex-1-enyl}propa-1,2-dienyl)phenyl]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

<1-D>-1-bromobutane (67402-19-1,148404-91-5) + acetic acid 3-{4-[bis-(4-bromophenyl)-amino]-phenyl}-1-{2-[(triisopropylsilanyl)-ethynyl]-cyclohex-1-enyl}-prop-2-ynyl ester (1173838-82-8) → bis-(4-bromophenyl)-[4-(1-(1-deuteriobutyl)-3-{2-[(triisopropylsilanyl)ethynyl]cyclohex-1-enyl}propa-1,2-dienyl)phenyl]-amine (1173838-55-5)

Guidance literature:

<1-D>-1-bromobutane; With magnesium; In tetrahydrofuran; Inert atmosphere;

With copper(l) iodide; lithium bromide; In tetrahydrofuran; at 0 ℃; for 0.25h; Inert atmosphere;

acetic acid 3-{4-[bis-(4-bromophenyl)-amino]-phenyl}-1-{2-[(triisopropylsilanyl)-ethynyl]-cyclohex-1-enyl}-prop-2-ynyl ester; In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere;

DOI:10.1021/jo900439x

Reference yield: 15.0%

bis-(4-bromophenyl)-[4-(1-(1-deuteriobutyl)-3-{2-[(triisopropylsilanyl)ethynyl]cyclohex-1-enyl}propa-1,2-dienyl)phenyl]-amine (1173838-55-5) → bis-(4-bromo-phenyl)-[10-(1-deuterio-butyl)-2,3,4,11-tetrahydro-1H-benzo[b]fluoren-7-yl]-amine + bis(4-bromophenyl)-(4-{1-deuterio[1-(1-triisopropylsilanyl-methylene)-4,5,6,7-tetrahydro-1H-inden-2-yl]-pent-1-enyl}-phenyl)-amine (1173838-60-2) + bis(4-bromophenyl)-[4-(2-deuterio-1-{1-[(triisopropylsilanyl)-methylene]-4,5,6,7-tetrahydro-1H-inden-2-yl}-pent-1-enyl)-phenyl]-amine (1173838-61-3)

Guidance literature:

With cyclohexa-1,4-diene; In toluene; for 7h; Inert atmosphere; Photolysis;

DOI:10.1021/jo900439x

Reference yield:

bis-(4-bromophenyl)-[4-(1-(1-deuteriobutyl)-3-{2-[(triisopropylsilanyl)ethynyl]cyclohex-1-enyl}propa-1,2-dienyl)phenyl]-amine (1173838-55-5) → bis(4-bromophenyl)-(4-{1-deuterio[1-(1-triisopropylsilanyl-methylene)-4,5,6,7-tetrahydro-1H-inden-2-yl]-pent-1-enyl}-phenyl)-amine (1173838-60-2) + bis(4-bromophenyl)-[4-(2-deuterio-1-{1-[(triisopropylsilanyl)-methylene]-4,5,6,7-tetrahydro-1H-inden-2-yl}-pent-1-enyl)-phenyl]-amine (1173838-61-3)

Guidance literature:

In toluene; for 48h; Inert atmosphere; Reflux;

DOI:10.1021/jo900439x

upstream raw materials:

<1-D>-1-bromobutane

acetic acid 3-{4-[bis-(4-bromophenyl)-amino]-phenyl}-1-{2-[(triisopropylsilanyl)-ethynyl]-cyclohex-1-enyl}-prop-2-ynyl ester

Downstream raw materials:

bis(4-bromophenyl)-(4-{1-deuterio[1-(1-triisopropylsilanyl-methylene)-4,5,6,7-tetrahydro-1H-inden-2-yl]-pent-1-enyl}-phenyl)-amine

bis(4-bromophenyl)-[4-(2-deuterio-1-{1-[(triisopropylsilanyl)-methylene]-4,5,6,7-tetrahydro-1H-inden-2-yl}-pent-1-enyl)-phenyl]-amine

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