5-(5-amino-2,4-bis-octyloxy-benzoylamino)-2,4-bis-octyloxy-benzoic acid methyl ester

Base Information

• Chemical Name: 5-(5-amino-2,4-bis-octyloxy-benzoylamino)-2,4-bis-octyloxy-benzoic acid methyl ester
• CAS No.: 916983-49-8
• Molecular Formula: C₄₇H₇₈N₂O₇
• Molecular Weight: 783.146

Synonyms:5-(5-amino-2,4-bis-octyloxy-benzoylamino)-2,4-bis-octyloxy-benzoic acid methyl ester

Chemical Property of 5-(5-amino-2,4-bis-octyloxy-benzoylamino)-2,4-bis-octyloxy-benzoic acid methyl ester

Chemical Property:

Purity/Quality:

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Technology Process of 5-(5-amino-2,4-bis-octyloxy-benzoylamino)-2,4-bis-octyloxy-benzoic acid methyl ester

There total 3 articles about 5-(5-amino-2,4-bis-octyloxy-benzoylamino)-2,4-bis-octyloxy-benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

5-(5-nitro-2,4-bis-octyloxy-benzoylamino)-2,4-bis-octyloxy-benzoic acid methyl ester (916983-47-6) → 5-(5-amino-2,4-bis-octyloxy-benzoylamino)-2,4-bis-octyloxy-benzoic acid methyl ester (916983-49-8)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; dichloromethane; at 20 ℃; for 6h; under 760 Torr;

DOI:10.1016/j.tet.2006.09.046

Reference yield:

2,4-dioctyloxy-5-nitrobenzoyl chloride (271261-75-7) → 5-(5-amino-2,4-bis-octyloxy-benzoylamino)-2,4-bis-octyloxy-benzoic acid methyl ester (916983-49-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 80 percent / triethylamine / CH₂Cl₂ / 4 h / 20 °C

2: 96 percent / hydrogen / Pd/C / CH₂Cl₂; methanol / 6 h / 20 °C / 760 Torr

With hydrogen; triethylamine; palladium on activated charcoal; In methanol; dichloromethane;

DOI:10.1016/j.tet.2006.09.046

Reference yield:

5-amino-2,4-bis-octyloxy-benzoic acid methyl ester → 5-(5-amino-2,4-bis-octyloxy-benzoylamino)-2,4-bis-octyloxy-benzoic acid methyl ester (916983-49-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 80 percent / triethylamine / CH₂Cl₂ / 4 h / 20 °C

2: 96 percent / hydrogen / Pd/C / CH₂Cl₂; methanol / 6 h / 20 °C / 760 Torr

With hydrogen; triethylamine; palladium on activated charcoal; In methanol; dichloromethane;

DOI:10.1016/j.tet.2006.09.046

upstream raw materials:

5-(5-nitro-2,4-bis-octyloxy-benzoylamino)-2,4-bis-octyloxy-benzoic acid methyl ester

2,4-dioctyloxy-5-nitrobenzoyl chloride

Downstream raw materials:

N,N-diethyl-N'-{5-[5-(5-imidazol-1-yl-2-octyloxy-phenylcarbamoyl)-2,4-bis-octyloxy-phenylcarbamoyl]-2,4-bis-octyloxy-phenyl}-malonamide

N-{5-[2,4-bis-octyloxy-5-(4-octyloxy-pyridin-3-ylcarbamoyl)-phenylcarbamoyl]-2,4-bis-octyloxy-phenyl}-N',N'-diethyl-malonamide

5-[5-(2-diethylcarbamoyl-acetylamino)-2,4-bis-octyloxy-benzoylamino]-2,4-bis-octyloxy-benzoic acid

5-[5-(2-diethylcarbamoyl-acetylamino)-2,4-bis-octyloxy-benzoylamino]-2,4-bis-octyloxy-benzoic acid methyl ester

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