benzyl N₂,N₂-bis(tert-butoxycarbonyl)-5-(2,3-dichlorophenyl)-D-lysinate

Base Information

• Chemical Name: benzyl N₂,N₂-bis(tert-butoxycarbonyl)-5-(2,3-dichlorophenyl)-D-lysinate
• CAS No.: 784156-15-6
• Molecular Formula: C₂₉H₃₈Cl₂N₂O₆
• Molecular Weight: 581.537

Synonyms:benzyl N₂,N₂-bis(tert-butoxycarbonyl)-5-(2,3-dichlorophenyl)-D-lysinate

Chemical Property of benzyl N₂,N₂-bis(tert-butoxycarbonyl)-5-(2,3-dichlorophenyl)-D-lysinate

Chemical Property:

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Technology Process of benzyl N₂,N₂-bis(tert-butoxycarbonyl)-5-(2,3-dichlorophenyl)-D-lysinate

There total 1 articles about benzyl N₂,N₂-bis(tert-butoxycarbonyl)-5-(2,3-dichlorophenyl)-D-lysinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl N,N-bis(tert-butoxycarbonyl)-5-(2,3-dichlorophenyl)-6-nitro-D-norleucinate (784156-13-4) → benzyl N2,N2-bis(tert-butoxycarbonyl)-5-(2,3-dichlorophenyl)-D-lysinate (784156-15-6)

Guidance literature:

With hydrogen; nickel; In ethanol; for 2h;

Reference yield:

benzyl N2,N2-bis(tert-butoxycarbonyl)-5-(2,3-dichlorophenyl)-D-lysinate (784156-15-6) → di-tert-butyl [(3R)-6-(2,3-dichlorophenyl)-2-oxoazepan-3-yl]imidobicarbonate

Guidance literature:

benzyl N₂,N₂-bis(tert-butoxycarbonyl)-5-(2,3-dichlorophenyl)-D-lysinate; With sodium hydroxide; water; In methanol; at 40 ℃; for 6h;

With hydrogenchloride; In methanol; water;

With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; for 2h; Alkaline aqueous solution;

upstream raw materials:

benzyl N,N-bis(tert-butoxycarbonyl)-5-(2,3-dichlorophenyl)-6-nitro-D-norleucinate

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