(1aR,5R,6S,7R,7aS,7bS)-6,7-bis(benzyloxy)-5-(tert-butyldimethylsilyloxy)octahydrooxireno[2,3-a]indolizine

Base Information

• Chemical Name: (1aR,5R,6S,7R,7aS,7bS)-6,7-bis(benzyloxy)-5-(tert-butyldimethylsilyloxy)octahydrooxireno[2,3-a]indolizine
• CAS No.: 1204748-38-8
• Molecular Formula: C₂₈H₃₉NO₄Si
• Molecular Weight: 481.707

Synonyms:(1aR,5R,6S,7R,7aS,7bS)-6,7-bis(benzyloxy)-5-(tert-butyldimethylsilyloxy)octahydrooxireno[2,3-a]indolizine

Chemical Property of (1aR,5R,6S,7R,7aS,7bS)-6,7-bis(benzyloxy)-5-(tert-butyldimethylsilyloxy)octahydrooxireno[2,3-a]indolizine

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Technology Process of (1aR,5R,6S,7R,7aS,7bS)-6,7-bis(benzyloxy)-5-(tert-butyldimethylsilyloxy)octahydrooxireno[2,3-a]indolizine

There total 1 articles about (1aR,5R,6S,7R,7aS,7bS)-6,7-bis(benzyloxy)-5-(tert-butyldimethylsilyloxy)octahydrooxireno[2,3-a]indolizine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

(2R,3R,4R)-3,4-bis(benzyloxy)-4-((1S,2S,5R)-6-oxa-3-azabicyclo[3.1.0]hexan-2-yl)-1-(tert-butyldimethylsilyloxy)butan-2-ol (1204748-36-6) → (1aR,4S,5R,6R,6bS)-5,6-bis(benzyloxy)-4-((tert-butyldimethylsilyloxy)methyl)hexahydro-1aH-oxireno[2,3-a]pyrrolizine (1204748-37-7) + (1aR,5R,6S,7R,7aS,7bS)-6,7-bis(benzyloxy)-5-(tert-butyldimethylsilyloxy)octahydrooxireno[2,3-a]indolizine (1204748-38-8)

Guidance literature:

With di-isopropyl azodicarboxylate; triphenylphosphine; In toluene; at 0 - 80 ℃;

DOI:10.1021/jo902355p

upstream raw materials:

(2R,3R,4R)-3,4-bis(benzyloxy)-4-((1S,2S,5R)-6-oxa-3-azabicyclo[3.1.0]hexan-2-yl)-1-(tert-butyldimethylsilyloxy)butan-2-ol

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