[Os(N-((pyridin-2-yl)benzylidene)aniline)(quinoline-8-olate)2](ClO₄)

Base Information

Chemical Name:[Os(N-((pyridin-2-yl)benzylidene)aniline)(quinoline-8-olate)2](ClO₄)
CAS No.:678140-51-7
Molecular Formula:C₃₆H₂₆N₄O₂Os*ClO₄
Molecular Weight:836.279
Hs Code.:

[Os(N-((pyridin-2-yl)benzylidene)aniline)(quinoline-8-olate)2](ClO<sub>4</sub>)

Synonyms:[Os(N-((pyridin-2-yl)benzylidene)aniline)(quinoline-8-olate)2](ClO₄)

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Chemical Property of [Os(N-((pyridin-2-yl)benzylidene)aniline)(quinoline-8-olate)2](ClO₄)

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Technology Process of [Os(N-((pyridin-2-yl)benzylidene)aniline)(quinoline-8-olate)2](ClO₄)

There total 2 articles about [Os(N-((pyridin-2-yl)benzylidene)aniline)(quinoline-8-olate)2](ClO₄) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: [Os(N-((pyridin-2-yl)benzylidene)aniline)(quinoline-8-olate)2](ClO₄)2

: 678140-51-7
[Os(N-((pyridin-2-yl)benzylidene)aniline)(quinoline-8-olate)2](ClO₄)

Guidance literature:: With N₂H₄*H₂O; In acetonitrile; dropwise addn. of soln. of N2H4*H2O (0.15 mmol) in CH3CN to soln. of Os-compd. (0.1 mmol) in CH3CN at 298 K under stirring; evapn. under reduced pressure, residue extd. with CH2Cl2, slow evapn., recrystn. from CH3CN/H2O, dried under vac. over P4O10;

Reference yield: 68.0%

: 30894-24-7
N-(phenyl(pyridin-2-yl)methylene)aniline

: 111267-27-7
[OsBr₂(quinoline-8-olate)2]

: sodium perchlorate

: 678140-51-7
[Os(N-((pyridin-2-yl)benzylidene)aniline)(quinoline-8-olate)2](ClO₄)

Guidance literature:: With 2-methoxyethanol; In 2-methoxy-ethanol; water; aniline deriv. added to suspn. of Os-compd. in MeOCH2CH2OH/H2O (2/1), heated under reflux for 6 h, soln. evapd. under vac., residue washed with ether, dried under vac., dissolved in satd. soln. of NaClO4 in EtOH/H2O,slowly evapd. on air; dissolved in CH2Cl2, chromy. (silica gel, CH2Cl2, then C6H6/MeCN (4/1)),slow evapn.; elem. anal.;

Reference yield: 60.0%

: 678140-51-7
[Os(N-((pyridin-2-yl)benzylidene)aniline)(quinoline-8-olate)2](ClO₄)

: sodium perchlorate

: [Os(N-((pyridin-2-yl)benzylidene)aniline)(quinoline-8-olate)2](ClO₄)2

Guidance literature:: With Ce(SO₄)2*4H₂O; In dichloromethane; sulfuric acid; acetonitrile; aq. H2SO4; soln. of Ce(IV) salt in 1M H2SO4 added dropwise to soln. of Os-compd. inCH2Cl2/MeCN (1/1) at 298 K under stirring, stirred for 15 min, filtered , evapd. under vac., dried, extn. with CH2Cl2, evapn. in air, solid dissolved in MeCN, aq. NaClO4 added; concd., stored overnight in refrigerator, ppt. filtered off, washed withcold water, dried under vac. over P4O10; elem. anal.;