3,4-bis-prop-2-ynyloxybenzoic acid ethyl ester

Base Information

Chemical Name:3,4-bis-prop-2-ynyloxybenzoic acid ethyl ester
CAS No.:618907-65-6
Molecular Formula:C₁₅H₁₄O₄
Molecular Weight:258.274
Hs Code.:

Synonyms:3,4-bis-prop-2-ynyloxybenzoic acid ethyl ester

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Chemical Property of 3,4-bis-prop-2-ynyloxybenzoic acid ethyl ester

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Technology Process of 3,4-bis-prop-2-ynyloxybenzoic acid ethyl ester

There total 1 articles about 3,4-bis-prop-2-ynyloxybenzoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 3943-89-3
Ethyl protocatechuate

: 106-96-7
propargyl bromide

: 618907-65-6
3,4-bis-prop-2-ynyloxybenzoic acid ethyl ester

Guidance literature:: With potassium carbonate; In acetone; at 50 ℃; Inert atmosphere;
DOI:10.1039/c7nj00225d

Reference yield: 86.0%

: 618907-65-6
3,4-bis-prop-2-ynyloxybenzoic acid ethyl ester

: (3,4-bis(prop-2-yn-1-yloxy)phenyl)methanol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 20 ℃; for 12h; Inert atmosphere;
DOI:10.3390/molecules25051088

Reference yield: 72.0%

: C₃₇H₆₇N₃O₃

: 618907-65-6
3,4-bis-prop-2-ynyloxybenzoic acid ethyl ester

: C₈₉H₁₄₈N₆O₁₀

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; In tetrahydrofuran; water; tert-butyl alcohol; at 25 ℃; for 20h;
DOI:10.1039/c7nj00225d