C₄₄H₅₅N₃O₁₃S

Base Information

Chemical Name:C₄₄H₅₅N₃O₁₃S
CAS No.:141823-82-7
Molecular Formula:C₄₄H₅₅N₃O₁₃S
Molecular Weight:865.999
Hs Code.:

C<sub>44</sub>H<sub>55</sub>N<sub>3</sub>O<sub>13</sub>S

Synonyms:C₄₄H₅₅N₃O₁₃S

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Chemical Property of C₄₄H₅₅N₃O₁₃S

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Technology Process of C₄₄H₅₅N₃O₁₃S

There total 14 articles about C₄₄H₅₅N₃O₁₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 141823-81-6
C₅₀H₆₉N₃O₁₃SSi

: 141823-82-7
C₄₄H₅₅N₃O₁₃S

Guidance literature:: With pyridine hydrogenfluoride; In tetrahydrofuran; dichloromethane; at -20 - 0 ℃; for 3h;

Reference yield:

: 126900-87-6
3-Chloro-benzoic acid (2S,3R,6R)-2-aminooxy-4-(tert-butyl-dimethyl-silanyloxy)-6-methyl-3,6-dihydro-2H-pyran-3-yl ester

: 141823-82-7
C₄₄H₅₅N₃O₁₃S

Guidance literature:: Multi-step reaction with 9 steps

1: 70 percent / pyridinium p-toluenesulfonate / benzene / 3 h / 25 °C

2: 100 percent / 2,6-lutidine / CH₂Cl₂ / 0.5 h / 0 to 25 deg C

3: 95 percent / i-Bu₂AlH / CH₂Cl₂ / 0.5 h / -78 °C

4: 86 percent / acetonitrile / 1.5 h / 25 °C

5: 100 percent / toluene / 1 h / 100 °C

6: 95 percent / NaSMe, EtSH / CH₂Cl₂ / 1.5 h / 25 °C

7: 90 percent / i-Pr₂EtN / CH₂Cl₂ / 1 h / 25 °C

8: 1.) AcOH, n-Bu₄NF, 2.) K-Selectride / 1.) THF, -40 to 0 deg C, 2.) DME, THF, -78 deg C, 0.7 h

9: 85 percent / HF*py / CH₂Cl₂; tetrahydrofuran / 3 h / -20 - 0 °C

With 2,6-dimethylpyridine; tetrabutyl ammonium fluoride; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; potassium tri-sec-butyl-borohydride; pyridine hydrogenfluoride; acetic acid; N-ethyl-N,N-diisopropylamine; ethanethiol; sodium thiomethoxide; In tetrahydrofuran; dichloromethane; toluene; acetonitrile; benzene;

Reference yield:

: 132938-43-3
(3aS,4R,6R,7R,7aR)-7-Hydroxy-4-methyl-6-(2-nitro-benzyloxy)-tetrahydro-[1,3]dioxolo[4,5-c]pyran-2-one

: 141823-82-7
C₄₄H₅₅N₃O₁₃S

Guidance literature:: Multi-step reaction with 12 steps

1: AgClO₄, SnCl₂, molecular sieves (4 Angstroem) / tetrahydrofuran / 7 h / -78 - -20 °C

2: NaH / tetrahydrofuran; ethane-1,2-diol / 0.5 h / 25 °C

3: 1.) n-Bu₂SnO, 2.) n-Bu₃SnOMe, Br₂ / 1.) MeOH, reflux, 1.2 h, 2.) CH₂Cl₂, 25 deg C

4: 70 percent / pyridinium p-toluenesulfonate / benzene / 3 h / 25 °C

5: 100 percent / 2,6-lutidine / CH₂Cl₂ / 0.5 h / 0 to 25 deg C

6: 95 percent / i-Bu₂AlH / CH₂Cl₂ / 0.5 h / -78 °C

7: 86 percent / acetonitrile / 1.5 h / 25 °C

8: 100 percent / toluene / 1 h / 100 °C

9: 95 percent / NaSMe, EtSH / CH₂Cl₂ / 1.5 h / 25 °C

10: 90 percent / i-Pr₂EtN / CH₂Cl₂ / 1 h / 25 °C

11: 1.) AcOH, n-Bu₄NF, 2.) K-Selectride / 1.) THF, -40 to 0 deg C, 2.) DME, THF, -78 deg C, 0.7 h

12: 85 percent / HF*py / CH₂Cl₂; tetrahydrofuran / 3 h / -20 - 0 °C

With 2,6-dimethylpyridine; 4 A molecular sieve; tetrabutyl ammonium fluoride; bromine; tributyltin methoxide; silver perchlorate; pyridinium p-toluenesulfonate; sodium hydride; diisobutylaluminium hydride; di(n-butyl)tin oxide; potassium tri-sec-butyl-borohydride; pyridine hydrogenfluoride; acetic acid; N-ethyl-N,N-diisopropylamine; ethanethiol; tin(ll) chloride; sodium thiomethoxide; In tetrahydrofuran; dichloromethane; ethylene glycol; toluene; acetonitrile; benzene;