2-(2-methoxy-4-n-pentylphenyl)-4-methylcyclohexaneacetic acid

Base Information

Chemical Name:2-(2-methoxy-4-n-pentylphenyl)-4-methylcyclohexaneacetic acid
CAS No.:133301-55-0
Molecular Formula:C₂₁H₃₂O₃
Molecular Weight:332.483
Hs Code.:

Synonyms:2-(2-methoxy-4-n-pentylphenyl)-4-methylcyclohexaneacetic acid

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Chemical Property of 2-(2-methoxy-4-n-pentylphenyl)-4-methylcyclohexaneacetic acid

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Technology Process of 2-(2-methoxy-4-n-pentylphenyl)-4-methylcyclohexaneacetic acid

There total 14 articles about 2-(2-methoxy-4-n-pentylphenyl)-4-methylcyclohexaneacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 133301-54-9
1-methyl-4-carboxymethyl-5-(2-methoxy-4-n-pentylphenyl)-cyclohex-1-ene

: 133301-55-0
2-(2-methoxy-4-n-pentylphenyl)-4-methylcyclohexaneacetic acid

Guidance literature:: With hydrogen; platinum(IV) oxide; In methanol; for 6h; under 2585.7 Torr;

Reference yield:

: 60441-58-9
2-hydroxy-4-n-pentylacetophenone

: 133301-55-0
2-(2-methoxy-4-n-pentylphenyl)-4-methylcyclohexaneacetic acid

Guidance literature:: Multi-step reaction with 11 steps

1: 85 percent / potassium carbonate / acetone / 12 h / Heating

2: 79.3 percent / NaOBr / H₂O; bis-(2-methoxy-ethyl) ether / 30 - 40 °C

3: 85.5 percent / LAH / diethyl ether

4: 97.5 percent / pyridinium chlorochromate / CH₂Cl₂ / 0.25 h

5: 90 percent / pyridine, piperidine / 2 h / Heating

6: 59 percent / xylene / 48 h / 185 °C

7: 97 percent / LAH / diethyl ether

8: 50 percent / pyridine, p-toluenesulfonyl chloride / 3 h / Heating

9: 62 percent / dimethylsulfoxide / 4 h / 90 °C

10: 76 percent / KOH / bis-(2-hydroxy-ethyl) ether / 20 h / Heating

11: 100 percent / H₂ / PtO₂ / methanol / 6 h / 2585.7 Torr

With piperidine; pyridine; potassium hydroxide; lithium aluminium tetrahydride; sodium hypobromide; hydrogen; potassium carbonate; p-toluenesulfonyl chloride; pyridinium chlorochromate; platinum(IV) oxide; In methanol; diethyl ether; dichloromethane; diethylene glycol dimethyl ether; water; dimethyl sulfoxide; acetone; xylene; diethylene glycol;

Reference yield:

: 20056-66-0
3-pentyl phenol

: 133301-55-0
2-(2-methoxy-4-n-pentylphenyl)-4-methylcyclohexaneacetic acid

Guidance literature:: Multi-step reaction with 13 steps

1: 95 percent / pyridine / 4 h

2: 62.5 percent / aluminium chloride / 2.5 h / 165 °C

3: 85 percent / potassium carbonate / acetone / 12 h / Heating

4: 79.3 percent / NaOBr / H₂O; bis-(2-methoxy-ethyl) ether / 30 - 40 °C

5: 85.5 percent / LAH / diethyl ether

6: 97.5 percent / pyridinium chlorochromate / CH₂Cl₂ / 0.25 h

7: 90 percent / pyridine, piperidine / 2 h / Heating

8: 59 percent / xylene / 48 h / 185 °C

9: 97 percent / LAH / diethyl ether

10: 50 percent / pyridine, p-toluenesulfonyl chloride / 3 h / Heating

11: 62 percent / dimethylsulfoxide / 4 h / 90 °C

12: 76 percent / KOH / bis-(2-hydroxy-ethyl) ether / 20 h / Heating

13: 100 percent / H₂ / PtO₂ / methanol / 6 h / 2585.7 Torr

With piperidine; pyridine; potassium hydroxide; lithium aluminium tetrahydride; aluminium trichloride; sodium hypobromide; hydrogen; potassium carbonate; p-toluenesulfonyl chloride; pyridinium chlorochromate; platinum(IV) oxide; In methanol; diethyl ether; dichloromethane; diethylene glycol dimethyl ether; water; dimethyl sulfoxide; acetone; xylene; diethylene glycol;