(1S*,8R*,9S*,12R*)-10,11-Diphenyl-13-oxatetracyclo[6.4.1.0^2,7.0^9,12]trideca-2,4,6,10-tetraene

Base Information

• Chemical Name: (1S*,8R*,9S*,12R*)-10,11-Diphenyl-13-oxatetracyclo[6.4.1.0^2,7.0^9,12]trideca-2,4,6,10-tetraene
• CAS No.: 316173-31-6
• Molecular Formula: C₂₄H₁₈O
• Molecular Weight: 322.406

Synonyms:(1S*,8R*,9S*,12R*)-10,11-Diphenyl-13-oxatetracyclo[6.4.1.0^2,7.0^9,12]trideca-2,4,6,10-tetraene

Chemical Property of (1S*,8R*,9S*,12R*)-10,11-Diphenyl-13-oxatetracyclo[6.4.1.0^2,7.0^9,12]trideca-2,4,6,10-tetraene

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Technology Process of (1S*,8R*,9S*,12R*)-10,11-Diphenyl-13-oxatetracyclo[6.4.1.0^2,7.0^9,12]trideca-2,4,6,10-tetraene

There total 2 articles about (1S*,8R*,9S*,12R*)-10,11-Diphenyl-13-oxatetracyclo[6.4.1.0^2,7.0^9,12]trideca-2,4,6,10-tetraene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

1,4-dihydronaphthalene-1,4-epoxide (573-57-9) + diphenyl acetylene (501-65-5) → (1S*,8R*,9S*,12R*)-10,11-Diphenyl-13-oxatetracyclo[6.4.1.02,7.09,12]trideca-2,4,6,10-tetraene (316173-31-6)

Guidance literature:

With chloro(cyclopentadienyl)bis(triphenylphosphine)ruthenium (II); methyl iodide; In 1,4-dioxane; diastereoselective reaction; Inert atmosphere; Heating;

DOI:10.1002/anie.201104589

Reference yield: 88.0%

1,4-dihydronaphthalene-1,4-epoxide (573-57-9) + diphenyl acetylene (501-65-5) → C20H16O2 + (1S*,8R*,9S*,12R*)-10,11-Diphenyl-13-oxatetracyclo[6.4.1.02,7.09,12]trideca-2,4,6,10-tetraene (316173-31-6)

Guidance literature:

With triphenylphosphine; zinc; diiodobis(triphenylphosphine)cobalt(II); In toluene; at 90 ℃; for 24h;

DOI:10.1021/jo010609y

Reference yield: 85.0%

(1S*,8R*,9S*,12R*)-10,11-Diphenyl-13-oxatetracyclo[6.4.1.02,7.09,12]trideca-2,4,6,10-tetraene (316173-31-6) → (1R*,8S*)-10,11-Diphenyl-13-oxatricyclo[6.4.1.02,7]trideca-2,4,6,9,11-pentaene

Guidance literature:

at 500 ℃; under 0.1 Torr;

DOI:10.1002/1521-3765(20001016)6:20<3706::AID-CHEM3706>3.0.CO;2-P

upstream raw materials:

1,4-dihydronaphthalene-1,4-epoxide

diphenyl acetylene

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