o-aminoazoxybenzene

Base Information

Chemical Name:o-aminoazoxybenzene
CAS No.:99137-34-5
Molecular Formula:C₁₂H₁₁N₃O
Molecular Weight:213.239
Hs Code.:

Synonyms:o-aminoazoxybenzene

Suppliers and Price of o-aminoazoxybenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of o-aminoazoxybenzene

Chemical Property:

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Technology Process of o-aminoazoxybenzene

There total 5 articles about o-aminoazoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 99137-33-4
2-phenyl-1,2,4-benzotriazin-3-one 1-oxide

: 1916-72-9
2-phenyl-2H-1,2,3-benzotriazole

: 99137-34-5
o-aminoazoxybenzene

Guidance literature:: With potassium hydroxide; In water; at 100 ℃; for 0.0833333h;

Reference yield:

: 728-90-5
N-(2-nitrophenyl)benzanilide

: 99137-34-5
o-aminoazoxybenzene

Guidance literature:: Multi-step reaction with 5 steps

1: phosphorus pentachloride / toluene / Ambient temperature

2: 81 percent / hydroxylamine / 1,2-dimethoxy-ethane; diethyl ether / 26 h / Ambient temperature

3: 67 percent / thionyl chloride / benzene / 1 h / Ambient temperature

4: 51 percent / toluene / 3 h / Heating

5: 71 percent / 10percent potassium hydroxide / H₂O / 0.08 h / 100 °C

With potassium hydroxide; thionyl chloride; phosphorus pentachloride; hydroxylamine; In 1,2-dimethoxyethane; diethyl ether; water; toluene; benzene;

Reference yield:

: 3493-72-9
N-(2-nitro-phenyl)-benzimidoyl chloride

: 99137-34-5
o-aminoazoxybenzene

Guidance literature:: Multi-step reaction with 4 steps

1: 81 percent / hydroxylamine / 1,2-dimethoxy-ethane; diethyl ether / 26 h / Ambient temperature

2: 67 percent / thionyl chloride / benzene / 1 h / Ambient temperature

3: 51 percent / toluene / 3 h / Heating

4: 71 percent / 10percent potassium hydroxide / H₂O / 0.08 h / 100 °C

With potassium hydroxide; thionyl chloride; hydroxylamine; In 1,2-dimethoxyethane; diethyl ether; water; toluene; benzene;