(4S,5R)-4-allyl-3-benzyl-5-((S)-2-(benzyloxy)-1-hydroxybut-3-en-2-yl)oxazolidin-2-one

Base Information

Chemical Name:(4S,5R)-4-allyl-3-benzyl-5-((S)-2-(benzyloxy)-1-hydroxybut-3-en-2-yl)oxazolidin-2-one
CAS No.:1337554-58-1
Molecular Formula:C₂₄H₂₇NO₄
Molecular Weight:393.483
Hs Code.:

Synonyms:(4S,5R)-4-allyl-3-benzyl-5-((S)-2-(benzyloxy)-1-hydroxybut-3-en-2-yl)oxazolidin-2-one

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Chemical Property of (4S,5R)-4-allyl-3-benzyl-5-((S)-2-(benzyloxy)-1-hydroxybut-3-en-2-yl)oxazolidin-2-one

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Technology Process of (4S,5R)-4-allyl-3-benzyl-5-((S)-2-(benzyloxy)-1-hydroxybut-3-en-2-yl)oxazolidin-2-one

There total 8 articles about (4S,5R)-4-allyl-3-benzyl-5-((S)-2-(benzyloxy)-1-hydroxybut-3-en-2-yl)oxazolidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.8%

: 1337554-53-6
benzyl N-benzyl-((4S,5R,6S)-6-(benzyloxy)-5-hydroxy-6-(hydroxymethyl)octa-1,7-dien-4-yl)carbamate

: 1337554-58-1
(4S,5R)-4-allyl-3-benzyl-5-((S)-2-(benzyloxy)-1-hydroxybut-3-en-2-yl)oxazolidin-2-one

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 20 ℃; for 0.333333h; Inert atmosphere;
DOI:10.1016/j.tetasy.2011.07.015

Reference yield:

: C₃₁H₃₃NO₅

: 1337554-58-1
(4S,5R)-4-allyl-3-benzyl-5-((S)-2-(benzyloxy)-1-hydroxybut-3-en-2-yl)oxazolidin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C

2: sodium hydride / tetrahydrofuran / 0.33 h / 20 °C / Inert atmosphere

With sodium tetrahydroborate; sodium hydride; In tetrahydrofuran; methanol;
DOI:10.1016/j.tetasy.2011.07.015

Reference yield:

: 1337554-26-3
C₂₇H₃₃NO₄

: 1337554-58-1
(4S,5R)-4-allyl-3-benzyl-5-((S)-2-(benzyloxy)-1-hydroxybut-3-en-2-yl)oxazolidin-2-one

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydrogencarbonate / 4 h / 0 - 20 °C

2: water; trifluoroacetic acid / 0 - 20 °C

3: sodium periodate / methanol; water / 4 h / 0 - 20 °C

4: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C

5: sodium hydride / tetrahydrofuran / 0.33 h / 20 °C / Inert atmosphere

With sodium tetrahydroborate; sodium periodate; water; sodium hydride; sodium hydrogencarbonate; trifluoroacetic acid; In tetrahydrofuran; methanol; water;
DOI:10.1016/j.tetasy.2011.07.015