N-(4-phenoxybenzenesulfonyl)-N-{[2-(4-sulfamoylphenyl)ethylcarbamoyl]methyl}-O-benzyl-D-valine

Base Information

Chemical Name:N-(4-phenoxybenzenesulfonyl)-N-{[2-(4-sulfamoylphenyl)ethylcarbamoyl]methyl}-O-benzyl-D-valine
CAS No.:1092691-02-5
Molecular Formula:C₃₄H₃₇N₃O₈S₂
Molecular Weight:679.815
Hs Code.:

Synonyms:N-(4-phenoxybenzenesulfonyl)-N-{[2-(4-sulfamoylphenyl)ethylcarbamoyl]methyl}-O-benzyl-D-valine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(4-phenoxybenzenesulfonyl)-N-{[2-(4-sulfamoylphenyl)ethylcarbamoyl]methyl}-O-benzyl-D-valine

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Technology Process of N-(4-phenoxybenzenesulfonyl)-N-{[2-(4-sulfamoylphenyl)ethylcarbamoyl]methyl}-O-benzyl-D-valine

There total 1 articles about N-(4-phenoxybenzenesulfonyl)-N-{[2-(4-sulfamoylphenyl)ethylcarbamoyl]methyl}-O-benzyl-D-valine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1092691-01-4
N-(4-phenoxybenzenesulfonyl)-N-hydroxycarbonylmethyl-O-benzyl-D-valine

: 35303-76-5
4-(2-aminoethyl)benzenesulfonamide

: 1092691-02-5
N-(4-phenoxybenzenesulfonyl)-N-{[2-(4-sulfamoylphenyl)ethylcarbamoyl]methyl}-O-benzyl-D-valine

Guidance literature:: N-(4-phenoxybenzenesulfonyl)-N-hydroxycarbonylmethyl-O-benzyl-D-valine; With 4-methyl-morpholine; chloroformic acid ethyl ester; In tetrahydrofuran; Cooling with ice;

4-(2-aminoethyl)benzenesulfonamide; In tetrahydrofuran; at 0 ℃; for 4h;
DOI:10.1021/jm800964f

Reference yield: 92.0%

: 1092691-02-5
N-(4-phenoxybenzenesulfonyl)-N-{[2-(4-sulfamoylphenyl)ethylcarbamoyl]methyl}-O-benzyl-D-valine

: 1092691-03-6
N-(4-phenoxybenzenesulfonyl)-N-{[2-(4-sulfamoylphenyl)ethylcarbamoyl]-methyl}-D-valine

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; for 3h; under 1125.11 Torr;
DOI:10.1021/jm800964f