Technology Process of C23H36N8O
There total 6 articles about C23H36N8O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C29H39N9O;
With
acetic acid;
In
water;
at 65 ℃;
With
sodium dithionite;
In
water;
at 65 ℃;
for 0.25h;
With
potassium carbonate;
In
water;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium methylate / methanol / 2 h / 55 °C
1.2: 0.5 h
2.1: hydrogenchloride; sodium nitrite / water
2.2: 0.5 h
3.1: N-ethyl-N,N-diisopropylamine; trichlorophosphate / 1 h / Reflux
4.1: dichloromethane / 1 h / 20 °C
4.2: 1.5 h / 45 °C
5.1: 0.25 h / 150 °C
6.1: acetic acid / water / 65 °C
6.2: 0.25 h / 65 °C
With
hydrogenchloride; sodium methylate; acetic acid; N-ethyl-N,N-diisopropylamine; sodium nitrite; trichlorophosphate;
In
methanol; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: hydrogenchloride; sodium nitrite / water
1.2: 0.5 h
2.1: N-ethyl-N,N-diisopropylamine; trichlorophosphate / 1 h / Reflux
3.1: dichloromethane / 1 h / 20 °C
3.2: 1.5 h / 45 °C
4.1: 0.25 h / 150 °C
5.1: acetic acid / water / 65 °C
5.2: 0.25 h / 65 °C
With
hydrogenchloride; acetic acid; N-ethyl-N,N-diisopropylamine; sodium nitrite; trichlorophosphate;
In
dichloromethane; water;