Technology Process of C39H50N8O4Si
There total 12 articles about C39H50N8O4Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine; triphenylphosphine;
In
1,4-dioxane; water;
at 50 ℃;
for 1.5h;
DOI:10.1021/ol403154w
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: triethylamine / acetonitrile / 2 h
2.1: sodium t-butanolate / tetrahydrofuran / 0.75 h
3.1: sodium hydroxide / methanol; water / Cooling with ice
4.1: di-isopropyl azodicarboxylate / acetonitrile / 18 h / 20 °C
4.2: 0.17 h
5.1: 1H-imidazole / N,N-dimethyl-formamide / 0.42 h
6.1: triethylamine / dichloromethane / 0.33 h
7.1: triethylamine; triphenylphosphine / water; 1,4-dioxane / 1.5 h / 50 °C
With
1H-imidazole; di-isopropyl azodicarboxylate; triethylamine; triphenylphosphine; sodium hydroxide; sodium t-butanolate;
In
tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ol403154w
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium t-butanolate / tetrahydrofuran / 0.75 h
2.1: sodium hydroxide / methanol; water / Cooling with ice
3.1: di-isopropyl azodicarboxylate / acetonitrile / 18 h / 20 °C
3.2: 0.17 h
4.1: 1H-imidazole / N,N-dimethyl-formamide / 0.42 h
5.1: triethylamine / dichloromethane / 0.33 h
6.1: triethylamine; triphenylphosphine / water; 1,4-dioxane / 1.5 h / 50 °C
With
1H-imidazole; di-isopropyl azodicarboxylate; triethylamine; triphenylphosphine; sodium hydroxide; sodium t-butanolate;
In
tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ol403154w
