Adamantane-1,3-dicarboxylic acid bis-[(S)-2-((S)-2-benzyloxycarbonylamino-3-methyl-butyrylamino)-2-methoxycarbonyl-ethyl] ester

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Chemical Name:Adamantane-1,3-dicarboxylic acid bis-[(S)-2-((S)-2-benzyloxycarbonylamino-3-methyl-butyrylamino)-2-methoxycarbonyl-ethyl] ester
CAS No.:197707-05-4
Molecular Formula:C₄₆H₆₀N₄O₁₄
Molecular Weight:893.001
Hs Code.:

Synonyms:Adamantane-1,3-dicarboxylic acid bis-[(S)-2-((S)-2-benzyloxycarbonylamino-3-methyl-butyrylamino)-2-methoxycarbonyl-ethyl] ester

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Chemical Property of Adamantane-1,3-dicarboxylic acid bis-[(S)-2-((S)-2-benzyloxycarbonylamino-3-methyl-butyrylamino)-2-methoxycarbonyl-ethyl] ester

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Technology Process of Adamantane-1,3-dicarboxylic acid bis-[(S)-2-((S)-2-benzyloxycarbonylamino-3-methyl-butyrylamino)-2-methoxycarbonyl-ethyl] ester

There total 2 articles about Adamantane-1,3-dicarboxylic acid bis-[(S)-2-((S)-2-benzyloxycarbonylamino-3-methyl-butyrylamino)-2-methoxycarbonyl-ethyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 34078-88-1
methyl ((benzyloxy)carbonyl)-L-valyl-L-serinate

: adamantane-1,3-dicarbonyl dichloride

: 197707-05-4
Adamantane-1,3-dicarboxylic acid bis-[(S)-2-((S)-2-benzyloxycarbonylamino-3-methyl-butyrylamino)-2-methoxycarbonyl-ethyl] ester

Guidance literature:: With dmap; In dichloromethane; acetonitrile; for 12h; Ambient temperature;
DOI:10.1021/ja971517m

Reference yield:

: 39269-10-8
adamantane-1,3-dicarboxylic acid

: 197707-05-4
Adamantane-1,3-dicarboxylic acid bis-[(S)-2-((S)-2-benzyloxycarbonylamino-3-methyl-butyrylamino)-2-methoxycarbonyl-ethyl] ester

Guidance literature:: Multi-step reaction with 2 steps

1: 3 h / Heating

2: 90 percent / N,N-dimethyl-4-aminopyridine / CH₂Cl₂; acetonitrile / 12 h / Ambient temperature

With dmap; In dichloromethane; acetonitrile;
DOI:10.1021/ja971517m