methyl 3-O-benzyl-4,6-O-benzylidene-2-deoxy-3-C-ethyl-α-D-ribo-hexopyranoside

Base Information

Chemical Name:methyl 3-O-benzyl-4,6-O-benzylidene-2-deoxy-3-C-ethyl-α-D-ribo-hexopyranoside
CAS No.:114244-27-8
Molecular Formula:C₂₃H₂₈O₅
Molecular Weight:384.472
Hs Code.:

Synonyms:methyl 3-O-benzyl-4,6-O-benzylidene-2-deoxy-3-C-ethyl-α-D-ribo-hexopyranoside

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Chemical Property of methyl 3-O-benzyl-4,6-O-benzylidene-2-deoxy-3-C-ethyl-α-D-ribo-hexopyranoside

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Technology Process of methyl 3-O-benzyl-4,6-O-benzylidene-2-deoxy-3-C-ethyl-α-D-ribo-hexopyranoside

There total 1 articles about methyl 3-O-benzyl-4,6-O-benzylidene-2-deoxy-3-C-ethyl-α-D-ribo-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 63598-31-2
methyl 4,6-O-(R)-benzylidene-2-deoxy-α-D-erythrohexopyranosid-3-ulose

: 114244-27-8
methyl 3-O-benzyl-4,6-O-benzylidene-2-deoxy-3-C-ethyl-α-D-ribo-hexopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / Mg / diethyl ether / 2 h / 0 °C

2: 92 percent / sodium hydride, tetrabutylammonium iodide / tetrahydrofuran / 1.5 h / 55 °C

With tetra-(n-butyl)ammonium iodide; sodium hydride; magnesium; In tetrahydrofuran; diethyl ether;
DOI:10.1016/0008-6215(87)80119-2

Reference yield: 81.0%

: 114244-27-8
methyl 3-O-benzyl-4,6-O-benzylidene-2-deoxy-3-C-ethyl-α-D-ribo-hexopyranoside

: 3-O-benzyl-2-deoxy-3-C-ethyl-D-ribo-hexopyranose

Guidance literature:: With acetic acid; at 55 ℃; for 2h;
DOI:10.1016/0008-6215(87)80119-2

Reference yield:

: 114244-27-8
methyl 3-O-benzyl-4,6-O-benzylidene-2-deoxy-3-C-ethyl-α-D-ribo-hexopyranoside

: 114244-34-7
(2R,3R,4S)-4-benzyloxy-4-ethyl-1,2,3,6-hexanetetrol

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / 75percent acetic acid / 2 h / 55 °C

2: 267 mg / pyridine / 12 h / Ambient temperature

3: 87 percent / sodium borohydride / ethanol

With pyridine; sodium tetrahydroborate; acetic acid; In ethanol;
DOI:10.1016/0008-6215(87)80119-2