C₂₂H₃₆O₄

Base Information Edit

Chemical Name:C₂₂H₃₆O₄
CAS No.:1312543-68-2
Molecular Formula:C₂₂H₃₆O₄
Molecular Weight:364.525
Hs Code.:
Mol file:1312543-68-2.mol

C<sub>22</sub>H<sub>36</sub>O<sub>4</sub>

Synonyms:C₂₂H₃₆O₄

Suppliers and Price of C₂₂H₃₆O₄

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₂H₃₆O₄ Edit

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₂H₃₆O₄

There total 13 articles about C₂₂H₃₆O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1312543-67-1
C₂₂H₃₄O₄

: 1312543-68-2
C₂₂H₃₆O₄

Guidance literature:: With sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; at 0 - 20 ℃; for 4h;
DOI:10.1016/j.tetlet.2011.04.008

Reference yield:

: 910228-56-7
(2R)-2-[(4S,5S)-5-ethyl-2-(4-methoxyphenyl)-1,3-dioxan-4-yl]propan-1-ol

: 1312543-68-2
C₂₂H₃₆O₄

Guidance literature:: Multi-step reaction with 13 steps

1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 0.33 h / 50 °C

2: lithium chloride; lithium diisopropyl amide / tetrahydrofuran / 14 h / -78 - 20 °C

3: ammonia borane; lithium diisopropyl amide / tetrahydrofuran / 4 h / -78 - 20 °C

4: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 - 20 °C

5: diisobutylaluminium hydride / dichloromethane / 2 h / -40 - -10 °C

6: sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 1.5 h / 0 - 20 °C

7: sodium hexamethyldisilazane / tetrahydrofuran / 18 h / -78 - 20 °C

8: tetrabutyl ammonium fluoride / tetrahydrofuran / 10 h / 0 - 20 °C

9: sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 1.5 h / 0 - 20 °C

10: benzoic acid / toluene / 0.25 h / 90 °C

11: diisobutylaluminium hydride / dichloromethane / 1 h / -78 - 0 °C

12: titanium(IV) isopropylate; tert.-butylhydroperoxide; D-(-)-diisopropyl tartrate / dichloromethane / 6 h / 0 - 20 °C

13: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran / 4 h / 0 - 20 °C

With 1H-imidazole; 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; ammonia borane; tetrabutyl ammonium fluoride; iodine; sodium hexamethyldisilazane; sulfur trioxide pyridine complex; diisobutylaluminium hydride; D-(-)-diisopropyl tartrate; triphenylphosphine; sodium bis(2-methoxyethoxy)aluminium dihydride; benzoic acid; lithium chloride; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; toluene; 2: Myers alkylation reaction / 7: Wittig reaction / 10: Wittig reaction / 12: Sharpless epoxidation;
DOI:10.1016/j.tetlet.2011.04.008

Reference yield:

: 1312543-60-4
C₁₉H₃₀O₄

: 1312543-68-2
C₂₂H₃₆O₄

Guidance literature:: Multi-step reaction with 10 steps

1: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 - 20 °C

2: diisobutylaluminium hydride / dichloromethane / 2 h / -40 - -10 °C

3: sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 1.5 h / 0 - 20 °C

4: sodium hexamethyldisilazane / tetrahydrofuran / 18 h / -78 - 20 °C

5: tetrabutyl ammonium fluoride / tetrahydrofuran / 10 h / 0 - 20 °C

6: sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 1.5 h / 0 - 20 °C

7: benzoic acid / toluene / 0.25 h / 90 °C

8: diisobutylaluminium hydride / dichloromethane / 1 h / -78 - 0 °C

9: titanium(IV) isopropylate; tert.-butylhydroperoxide; D-(-)-diisopropyl tartrate / dichloromethane / 6 h / 0 - 20 °C

10: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran / 4 h / 0 - 20 °C

With 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; sulfur trioxide pyridine complex; diisobutylaluminium hydride; D-(-)-diisopropyl tartrate; sodium bis(2-methoxyethoxy)aluminium dihydride; benzoic acid; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; toluene; 4: Wittig reaction / 7: Wittig reaction / 9: Sharpless epoxidation;
DOI:10.1016/j.tetlet.2011.04.008