(3S,4R,5S)-5-dibenzylamino-3-dimethylphenylsilyl-7-methyl-1,4-octandiol

Base Information

Chemical Name:(3S,4R,5S)-5-dibenzylamino-3-dimethylphenylsilyl-7-methyl-1,4-octandiol
CAS No.:145064-10-4
Molecular Formula:C₃₁H₄₃NO₂Si
Molecular Weight:489.773
Hs Code.:

Synonyms:(3S,4R,5S)-5-dibenzylamino-3-dimethylphenylsilyl-7-methyl-1,4-octandiol

Suppliers and Price of (3S,4R,5S)-5-dibenzylamino-3-dimethylphenylsilyl-7-methyl-1,4-octandiol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (3S,4R,5S)-5-dibenzylamino-3-dimethylphenylsilyl-7-methyl-1,4-octandiol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (3S,4R,5S)-5-dibenzylamino-3-dimethylphenylsilyl-7-methyl-1,4-octandiol

There total 3 articles about (3S,4R,5S)-5-dibenzylamino-3-dimethylphenylsilyl-7-methyl-1,4-octandiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 136320-55-3
3-(dimethylphenylsilyl)-2-propynyl N,N-diisopropylcarbamate

: 145064-10-4
(3S,4R,5S)-5-dibenzylamino-3-dimethylphenylsilyl-7-methyl-1,4-octandiol

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / H₂, ethylenediamine / P-2 Ni / ethanol / Ambient temperature

3: 1.) Me₂S*BH₃, 2.) 30percent H₂O₂, 2N aq. NaOH / 1.) THF, 50 deg C, 4 h, 2.) EtOH, 2 h, reflux

With sodium hydroxide; dimethylsulfide borane complex; hydrogen; dihydrogen peroxide; ethylenediamine; P-2 Ni; In ethanol;
DOI:10.1055/s-1992-26247

Reference yield:

: 111060-65-2
(S)-2-(dibenzylamino)-4-methylpentanal

: 145064-10-4
(3S,4R,5S)-5-dibenzylamino-3-dimethylphenylsilyl-7-methyl-1,4-octandiol

Guidance literature:: Multi-step reaction with 2 steps

2: 1.) Me₂S*BH₃, 2.) 30percent H₂O₂, 2N aq. NaOH / 1.) THF, 50 deg C, 4 h, 2.) EtOH, 2 h, reflux

With sodium hydroxide; dimethylsulfide borane complex; dihydrogen peroxide;
DOI:10.1055/s-1992-26247

Reference yield:

: 145064-05-7
(Z)-3-dimethylphenylsilyl-2-propenyl N,N-diisopropylcarbamate

: 145064-10-4
(3S,4R,5S)-5-dibenzylamino-3-dimethylphenylsilyl-7-methyl-1,4-octandiol

Guidance literature:: Multi-step reaction with 2 steps

2: 1.) Me₂S*BH₃, 2.) 30percent H₂O₂, 2N aq. NaOH / 1.) THF, 50 deg C, 4 h, 2.) EtOH, 2 h, reflux

With sodium hydroxide; dimethylsulfide borane complex; dihydrogen peroxide;
DOI:10.1055/s-1992-26247