ethyl 4,6-O-benzylidene-2,3-dideoxy-3-iodo-2-(2,2,2-trichloroethoxycarbonylamino)-1-thio-β-D-allopyranoside

Base Information

Chemical Name:ethyl 4,6-O-benzylidene-2,3-dideoxy-3-iodo-2-(2,2,2-trichloroethoxycarbonylamino)-1-thio-β-D-allopyranoside
CAS No.:919078-12-9
Molecular Formula:C₁₈H₂₁Cl₃INO₅S
Molecular Weight:596.698
Hs Code.:

Synonyms:ethyl 4,6-O-benzylidene-2,3-dideoxy-3-iodo-2-(2,2,2-trichloroethoxycarbonylamino)-1-thio-β-D-allopyranoside

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Chemical Property of ethyl 4,6-O-benzylidene-2,3-dideoxy-3-iodo-2-(2,2,2-trichloroethoxycarbonylamino)-1-thio-β-D-allopyranoside

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Technology Process of ethyl 4,6-O-benzylidene-2,3-dideoxy-3-iodo-2-(2,2,2-trichloroethoxycarbonylamino)-1-thio-β-D-allopyranoside

There total 2 articles about ethyl 4,6-O-benzylidene-2,3-dideoxy-3-iodo-2-(2,2,2-trichloroethoxycarbonylamino)-1-thio-β-D-allopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1054630-79-3
ethyl 4,6-O-benzylidene-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-3-O-(trifluoromethylsulfonyl)-1-thio-β-D-glucopyranoside

: 919078-12-9
ethyl 4,6-O-benzylidene-2,3-dideoxy-3-iodo-2-(2,2,2-trichloroethoxycarbonylamino)-1-thio-β-D-allopyranoside

Guidance literature:: With sodium iodide; In 1,2-dimethoxyethane; at 20 ℃;
DOI:10.1002/ejoc.200600515

Reference yield:

: 219518-08-8
ethyl 4,6-O-benzylidene-2-deoxy-<<(2,2,2-trichloroethoxy)carbonyl>amino>-1-thio-β-D-glucopyranoside

: 919078-12-9
ethyl 4,6-O-benzylidene-2,3-dideoxy-3-iodo-2-(2,2,2-trichloroethoxycarbonylamino)-1-thio-β-D-allopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / CH₂Cl₂ / 0.5 h / 0 °C

2: 10.78 g / NaI / 1,2-dimethoxy-ethane / 20 °C

With pyridine; sodium iodide; In 1,2-dimethoxyethane; dichloromethane;
DOI:10.1002/ejoc.200600515