3-[7-oxo-4-(3-trifluoromethyl-phenyl)-[1,4]diazepan-1-yl]-propionaldehyde

Base Information

• Chemical Name: 3-[7-oxo-4-(3-trifluoromethyl-phenyl)-[1,4]diazepan-1-yl]-propionaldehyde
• CAS No.: 1206600-42-1
• Molecular Formula: C₁₅H₁₇F₃N₂O₂
• Molecular Weight: 314.307

Synonyms:3-[7-oxo-4-(3-trifluoromethyl-phenyl)-[1,4]diazepan-1-yl]-propionaldehyde

Chemical Property of 3-[7-oxo-4-(3-trifluoromethyl-phenyl)-[1,4]diazepan-1-yl]-propionaldehyde

Chemical Property:

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Technology Process of 3-[7-oxo-4-(3-trifluoromethyl-phenyl)-[1,4]diazepan-1-yl]-propionaldehyde

There total 1 articles about 3-[7-oxo-4-(3-trifluoromethyl-phenyl)-[1,4]diazepan-1-yl]-propionaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

4-but-3-enyl-1-(3-trifluoromethyl-phenyl)-[1,4]diazepan-5-one (1206600-41-0) → 3-[7-oxo-4-(3-trifluoromethyl-phenyl)-[1,4]diazepan-1-yl]-propionaldehyde (1206600-42-1)

Guidance literature:

With potassium osmate(VI) dihydrate; sodium periodate; In tert-butyl alcohol; for 1h;

Reference yield: 44.0%

4-hydroxy-4-phenylpiperidin (40807-61-2) + 3-[7-oxo-4-(3-trifluoromethyl-phenyl)-[1,4]diazepan-1-yl]-propionaldehyde (1206600-42-1) → 4-[3-(4-hydroxy-4-phenyl-piperidin-1-yl)-propyl]-1-(3-trifluoromethyl-phenyl)-[1,4]diazepan-5-one (1206600-40-9)

Guidance literature:

With pyridine; borane pyridine; acetic acid; In ethanol; 1,2-dichloro-ethane; for 16h;

upstream raw materials:

4-but-3-enyl-1-(3-trifluoromethyl-phenyl)-[1,4]diazepan-5-one

Downstream raw materials:

4-[3-(4-hydroxy-4-phenyl-piperidin-1-yl)-propyl]-1-(3-trifluoromethyl-phenyl)-[1,4]diazepan-5-one

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