3-(2-aminophenyl)-N-hexylmaleimide

Base Information

Chemical Name:3-(2-aminophenyl)-N-hexylmaleimide
CAS No.:1394920-37-6
Molecular Formula:C₁₆H₂₀N₂O₂
Molecular Weight:272.347
Hs Code.:

Synonyms:3-(2-aminophenyl)-N-hexylmaleimide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(2-aminophenyl)-N-hexylmaleimide

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Technology Process of 3-(2-aminophenyl)-N-hexylmaleimide

There total 2 articles about 3-(2-aminophenyl)-N-hexylmaleimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 185408-20-2
o-(tributylstannyl)aniline

: 1228144-44-2
N-hexyl bromomaleimide

: 1394920-37-6
3-(2-aminophenyl)-N-hexylmaleimide

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; triphenyl-arsane; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1016/j.tetlet.2012.06.138

Reference yield:

: 148493-54-3
tributyl (o-tert-butyloxycarbonylaminophenyl) stannane

: 1394920-37-6
3-(2-aminophenyl)-N-hexylmaleimide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 2,6-dimethylpyridine; trimethylsilyl trifluoromethanesulfonate / dichloromethane / 1 h / 20 °C / Inert atmosphere

1.2: 0.5 h / 20 °C / Inert atmosphere

2.1: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; triphenyl-arsane / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; triphenyl-arsane; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; N,N-dimethyl-formamide; 2.1: |Stille Cross-Coupling (Migita-Kosugi-Stille Coupling);
DOI:10.1016/j.tetlet.2012.06.138