C₇₂H₁₄₀Si₁₄

Base Information

• Chemical Name: C₇₂H₁₄₀Si₁₄
• CAS No.: 151545-05-0
• Molecular Formula: C₇₂H₁₄₀Si₁₄
• Molecular Weight: 1399.1
• Mol file: 151545-05-0.mol

Synonyms:C₇₂H₁₄₀Si₁₄

Chemical Property of C₇₂H₁₄₀Si₁₄

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₇₂H₁₄₀Si₁₄

There total 2 articles about C₇₂H₁₄₀Si₁₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C36H70Br2Si7 (151545-13-0) → C72H140Si14 (151545-05-0)

Guidance literature:

With naphthalen-1-yl-lithium; In tetrahydrofuran; at -78 ℃;

DOI:10.1021/ja00075a096

Reference yield:

(CH3)3C6H2[((CH3)3Si)2CH]3C6H2SiH2 (135139-77-4) → C72H140Si14 (151545-05-0)

Guidance literature:

Multi-step reaction with 2 steps

1: N-bromosuccinimide, benzoyl peroxide / benzene / 80 °C

2: lithium naphthalenide / tetrahydrofuran / -78 °C

With N-Bromosuccinimide; Perbenzoic acid; naphthalen-1-yl-lithium; In tetrahydrofuran; benzene;

DOI:10.1021/ja00075a096

Reference yield: 100.0%

triethylsilane (617-86-7) + C72H140Si14 (151545-05-0) → 2-<2,4,6-trisphenyl>-1,1,1-triethyl-2-mesityldisilane

Guidance literature:

In toluene; at 70 ℃;

DOI:10.1021/ja00075a096

upstream raw materials:

C₃₆H₇₀Br₂Si₇

(CH₃)3C₆H₂[((CH₃)3Si)2CH]3C₆H₂SiH₂

Downstream raw materials:

1,2,3,4,5-tetrathiasilolane