5-[{(1R,2S)-(2-hexylcyclopropyl)}methanesulfonyl]-1-phenyl-1H-tetrazole

Base Information

Chemical Name:5-[{(1R,2S)-(2-hexylcyclopropyl)}methanesulfonyl]-1-phenyl-1H-tetrazole
CAS No.:1042088-99-2
Molecular Formula:C₁₇H₂₄N₄O₂S
Molecular Weight:348.469
Hs Code.:

Synonyms:5-[{(1R,2S)-(2-hexylcyclopropyl)}methanesulfonyl]-1-phenyl-1H-tetrazole

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Chemical Property of 5-[{(1R,2S)-(2-hexylcyclopropyl)}methanesulfonyl]-1-phenyl-1H-tetrazole

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Technology Process of 5-[{(1R,2S)-(2-hexylcyclopropyl)}methanesulfonyl]-1-phenyl-1H-tetrazole

There total 8 articles about 5-[{(1R,2S)-(2-hexylcyclopropyl)}methanesulfonyl]-1-phenyl-1H-tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 5-({[(1R,2S)-2-hexylcyclopropyl]methyl}thio)-1-phenyl-1H-tetrazole

: 1042088-99-2
5-[{(1R,2S)-(2-hexylcyclopropyl)}methanesulfonyl]-1-phenyl-1H-tetrazole

Guidance literature:: With ammonium molybdate; dihydrogen peroxide; In tetrahydrofuran; ethanol; water; at 20 ℃;
DOI:10.1039/c4ob01863j

Reference yield:

: (4S)-4-benzyl-3-[(1R,2S)-2-hexylcyclopropane-1-carbonyl]oxazolidin-2-one

: 1042088-99-2
5-[{(1R,2S)-(2-hexylcyclopropyl)}methanesulfonyl]-1-phenyl-1H-tetrazole

Guidance literature:: Multi-step reaction with 3 steps

1: lithium borohydride; methanol / tetrahydrofuran / 4 h / 0 - 20 °C

2: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C / Molecular sieve

3: ammonium molybdate; dihydrogen peroxide / water; tetrahydrofuran; ethanol / 20 °C

With methanol; lithium borohydride; ammonium molybdate; di-isopropyl azodicarboxylate; dihydrogen peroxide; triphenylphosphine; In tetrahydrofuran; ethanol; water; 2: |Mitsunobu Displacement;
DOI:10.1039/c4ob01863j

Reference yield:

: 252009-90-8
(1R,2S)-2-hexyl-1-hydroxymethylcyclopropane

: 1042088-99-2
5-[{(1R,2S)-(2-hexylcyclopropyl)}methanesulfonyl]-1-phenyl-1H-tetrazole

Guidance literature:: Multi-step reaction with 2 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C / Molecular sieve

2: ammonium molybdate; dihydrogen peroxide / water; tetrahydrofuran; ethanol / 20 °C

With ammonium molybdate; di-isopropyl azodicarboxylate; dihydrogen peroxide; triphenylphosphine; In tetrahydrofuran; ethanol; water; 1: |Mitsunobu Displacement;
DOI:10.1039/c4ob01863j