Technology Process of 2,6-dibromo-4-(N,N-dimethylamino)aniline
There total 3 articles about 2,6-dibromo-4-(N,N-dimethylamino)aniline which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogenchloride; tin(II) chloride dihdyrate;
In
chloroform; water; isopropyl alcohol;
for 5h;
Reflux;
DOI:10.1021/om200193r
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate / methanol; dimethyl sulfoxide / 3.5 h / 20 °C
2: hydrogenchloride; tin(II) chloride dihdyrate / chloroform; water; isopropyl alcohol / 5 h / Reflux
With
hydrogenchloride; tin(II) chloride dihdyrate; potassium carbonate;
In
methanol; chloroform; water; dimethyl sulfoxide; isopropyl alcohol;
DOI:10.1021/om200193r
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 5 h / Reflux
1.2: 3 h / Reflux
2.1: potassium carbonate / methanol; dimethyl sulfoxide / 3.5 h / 20 °C
3.1: hydrogenchloride; tin(II) chloride dihdyrate / chloroform; water; isopropyl alcohol / 5 h / Reflux
With
hydrogenchloride; tin(II) chloride dihdyrate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid;
In
methanol; dichloromethane; chloroform; water; dimethyl sulfoxide; isopropyl alcohol;
DOI:10.1021/om200193r
