C₄₆H₆₅N₁₉

Base Information

• Chemical Name: C₄₆H₆₅N₁₉
• CAS No.: 370589-93-8
• Molecular Formula: C₄₆H₆₅N₁₉
• Molecular Weight: 884.149
• Mol file: 370589-93-8.mol

Synonyms:C₄₆H₆₅N₁₉

Chemical Property of C₄₆H₆₅N₁₉

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₆H₆₅N₁₉

There total 3 articles about C₄₆H₆₅N₁₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

(4-aminomethyl)aniline (4403-71-8) + C39H56ClN17 (370589-91-6) → C46H65N19 (370589-93-8)

Guidance literature:

In tetrahydrofuran; at 80 ℃; for 24h;

DOI:10.1021/ja0041369

Reference yield:

2-chloro-4,6-bis-(n-butylamino)-1,3,5-triazine (7386-43-8) → C46H65N19 (370589-93-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 96 percent / tetrahydrofuran / 12 h / 70 °C

2: 95 percent / DIPEA / tetrahydrofuran / 25 h / 0 - 20 °C

3: 92 percent / tetrahydrofuran / 24 h / 80 °C

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran;

DOI:10.1021/ja0041369

Reference yield:

N-(4-amino-benzyl)-N',N''-dibutyl-[1,3,5]triazine-2,4,6-triamine (370589-90-5) → C46H65N19 (370589-93-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 95 percent / DIPEA / tetrahydrofuran / 25 h / 0 - 20 °C

2: 92 percent / tetrahydrofuran / 24 h / 80 °C

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran;

DOI:10.1021/ja0041369

upstream raw materials:

(4-aminomethyl)aniline

C₃₉H₅₆ClN₁₇

2-chloro-4,6-bis-(n-butylamino)-1,3,5-triazine

N-(4-amino-benzyl)-N',N''-dibutyl-[1,3,5]triazine-2,4,6-triamine