[S,S]-N,N'-bis-[3-(benzyloxycarbonyl)-2-(N-t-butoxycarbonylamino)-propionyl]-2,7-diaza-1,2,3,6,7,8-hexahydropyrene

Base Information

Chemical Name:[S,S]-N,N'-bis-[3-(benzyloxycarbonyl)-2-(N-t-butoxycarbonylamino)-propionyl]-2,7-diaza-1,2,3,6,7,8-hexahydropyrene
CAS No.:828301-08-2
Molecular Formula:C₄₆H₅₂N₄O₁₀
Molecular Weight:820.94
Hs Code.:

Synonyms:[S,S]-N,N'-bis-[3-(benzyloxycarbonyl)-2-(N-t-butoxycarbonylamino)-propionyl]-2,7-diaza-1,2,3,6,7,8-hexahydropyrene

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Chemical Property of [S,S]-N,N'-bis-[3-(benzyloxycarbonyl)-2-(N-t-butoxycarbonylamino)-propionyl]-2,7-diaza-1,2,3,6,7,8-hexahydropyrene

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Technology Process of [S,S]-N,N'-bis-[3-(benzyloxycarbonyl)-2-(N-t-butoxycarbonylamino)-propionyl]-2,7-diaza-1,2,3,6,7,8-hexahydropyrene

There total 1 articles about [S,S]-N,N'-bis-[3-(benzyloxycarbonyl)-2-(N-t-butoxycarbonylamino)-propionyl]-2,7-diaza-1,2,3,6,7,8-hexahydropyrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7536-58-5,98482-77-0
BOC-L-aspartic acid 4-benzyl ester

: 118080-77-6
1,2,3,6,7,8-hexahydrobenzo[lmn][3,8]phenanthroline

: 828301-08-2
[S,S]-N,N'-bis-[3-(benzyloxycarbonyl)-2-(N-t-butoxycarbonylamino)-propionyl]-2,7-diaza-1,2,3,6,7,8-hexahydropyrene

Guidance literature:: With dmap; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; sodium hydrogencarbonate; In chloroform; at 20 ℃;
DOI:10.1055/s-2004-835633

Reference yield:

: 76-05-1
trifluoroacetic acid

: 828301-08-2
[S,S]-N,N'-bis-[3-(benzyloxycarbonyl)-2-(N-t-butoxycarbonylamino)-propionyl]-2,7-diaza-1,2,3,6,7,8-hexahydropyrene

: 3-amino-4-[7-(2-amino-3-benzyloxycarbonyl-propionyl)-3,6,7,8-tetrahydro-1H-benzo[lmn][3,8]phenanthrolin-2-yl]-4-oxo-butyric acid benzyl ester; compound with trifluoro-acetic acid

Guidance literature:: With triethylsilane; In dichloromethane; at 20 ℃;
DOI:10.1055/s-2004-835633

Reference yield:

: 828301-08-2
[S,S]-N,N'-bis-[3-(benzyloxycarbonyl)-2-(N-t-butoxycarbonylamino)-propionyl]-2,7-diaza-1,2,3,6,7,8-hexahydropyrene

: 828301-11-7
[S,S]-N,N'-bis-[3-(benzyloxycarbonyl)-2-(N-5-fluoro-2,4-dinitrophenylamino)-propionyl]-2,7-diaza-1,2,3,6,7,8-hexahydropyrene

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃SiH / CH₂Cl₂ / 20 °C

2: Cs₂CO₃ / tetrahydrofuran

With triethylsilane; caesium carbonate; In tetrahydrofuran; dichloromethane;
DOI:10.1055/s-2004-835633