2-bromobenzoyldideuterioacetonitrile

Base Information

Chemical Name:2-bromobenzoyldideuterioacetonitrile
CAS No.:295788-81-7
Molecular Formula:C₉H₆BrNO
Molecular Weight:226.041
Hs Code.:

Synonyms:2-bromobenzoyldideuterioacetonitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-bromobenzoyldideuterioacetonitrile

Chemical Property:

Purity/Quality:

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Technology Process of 2-bromobenzoyldideuterioacetonitrile

There total 2 articles about 2-bromobenzoyldideuterioacetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53882-80-7
3-(2-bromophenyl)-3-oxopropanenitrile

: 295788-81-7
2-bromobenzoyldideuterioacetonitrile

Guidance literature:: With tetrabutylammomium bromide; water-d2; In chloroform-d1; for 2h;
DOI:10.1021/jo991968k

Reference yield:

: 6091-64-1
2-bromobenzoic acid ethyl ester

: 295788-81-7
2-bromobenzoyldideuterioacetonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / NaH / tetrahydrofuran / Heating

2: D₂O; Bu₄NBr / CDCl₃ / 2 h

With tetrabutylammomium bromide; water-d2; sodium hydride; In tetrahydrofuran; chloroform-d1; 1: Condensation / 2: Substitution;
DOI:10.1021/jo991968k

Reference yield:

: 295788-81-7
2-bromobenzoyldideuterioacetonitrile

: 2-deuteriobenzoylacetonitrile

Guidance literature:: 2-bromobenzoyldideuterioacetonitrile; With tert.-butyl lithium; In tetrahydrofuran; at -78 - 20 ℃;

With water; Further stages.;
DOI:10.1021/jo991968k