benzyl {2-[4-(3-chloropropoxy)phenyl]-5,6-dihydro-4H-cyclopenta[d][1,3]thiazol-5-yl}carbamate

Base Information

Chemical Name:benzyl {2-[4-(3-chloropropoxy)phenyl]-5,6-dihydro-4H-cyclopenta[d][1,3]thiazol-5-yl}carbamate
CAS No.:1004764-72-0
Molecular Formula:C₂₃H₂₃ClN₂O₃S
Molecular Weight:442.966
Hs Code.:

Synonyms:benzyl {2-[4-(3-chloropropoxy)phenyl]-5,6-dihydro-4H-cyclopenta[d][1,3]thiazol-5-yl}carbamate

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Chemical Property of benzyl {2-[4-(3-chloropropoxy)phenyl]-5,6-dihydro-4H-cyclopenta[d][1,3]thiazol-5-yl}carbamate

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Technology Process of benzyl {2-[4-(3-chloropropoxy)phenyl]-5,6-dihydro-4H-cyclopenta[d][1,3]thiazol-5-yl}carbamate

There total 12 articles about benzyl {2-[4-(3-chloropropoxy)phenyl]-5,6-dihydro-4H-cyclopenta[d][1,3]thiazol-5-yl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 100-51-6,185532-71-2
benzyl alcohol

: 1004764-72-0
benzyl {2-[4-(3-chloropropoxy)phenyl]-5,6-dihydro-4H-cyclopenta[d][1,3]thiazol-5-yl}carbamate

Guidance literature:: 2-[4-(3-chloropropoxy)phenyl]-5,6-dihydro-4H-cyclopenta[1,3]thiazole-5-carboxylic acid; With diphenyl phosphoryl azide; triethylamine; In toluene; at 40 ℃;

benzyl alcohol; In toluene; at 90 ℃; for 24h;

Reference yield: 90.0%

: 2-[4-(3-chloropropoxy)phenyl]-5,6-dihydro-4H-cyclopenta[1,3]thiazole-5-carboxylic acid

: 100-51-6,185532-71-2
benzyl alcohol

: 1004764-72-0
benzyl {2-[4-(3-chloropropoxy)phenyl]-5,6-dihydro-4H-cyclopenta[d][1,3]thiazol-5-yl}carbamate

Guidance literature:: 2-[4-(3-chloropropoxy)phenyl]-5,6-dihydro-4H-cyclopenta[1,3]thiazole-5-carboxylic acid; With diphenyl phosphoryl azide; triethylamine; In toluene; at 20 ℃; for 12h;

benzyl alcohol; In toluene; for 24h; Reflux;
DOI:10.1002/cmdc.201100248

Reference yield:

: 58101-60-3
methyl cyclopent-3-ene-1-carboxylate

: 1004764-72-0
benzyl {2-[4-(3-chloropropoxy)phenyl]-5,6-dihydro-4H-cyclopenta[d][1,3]thiazol-5-yl}carbamate

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-Bromosuccinimide; water; calcium carbonate / acetonitrile / 4 h / 20 °C

2.1: Dess-Martin periodane / dichloromethane / 48 h / 20 °C

3.1: ethanol / 12 h / Reflux

4.1: water; lithium hydroxide / tetrahydrofuran / 12 h / 20 °C

5.1: diphenyl phosphoryl azide; triethylamine / toluene / 12 h / 20 °C

5.2: 24 h / Reflux

With N-Bromosuccinimide; diphenyl phosphoryl azide; water; Dess-Martin periodane; triethylamine; calcium carbonate; lithium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; toluene; acetonitrile; 3.1: Hantzsch condensation / 5.2: Curtius rearrangement;
DOI:10.1002/cmdc.201100248