C₆₅H₁₁₂N₁₀O₁₆

Base Information

Chemical Name:C₆₅H₁₁₂N₁₀O₁₆
CAS No.:1191932-85-0
Molecular Formula:C₆₅H₁₁₂N₁₀O₁₆
Molecular Weight:1289.66
Hs Code.:

C<sub>65</sub>H<sub>112</sub>N<sub>10</sub>O<sub>16</sub>

Synonyms:C₆₅H₁₁₂N₁₀O₁₆

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆₅H₁₁₂N₁₀O₁₆

Chemical Property:

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Technology Process of C₆₅H₁₁₂N₁₀O₁₆

There total 3 articles about C₆₅H₁₁₂N₁₀O₁₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1191932-84-9
C₁₃H₁₄Cl₂N₂O₄

: 4,7-bis-tertbutoxycarbonylmethyl-1,4,7,10-tetraazacyclododec-1-yl acetic acid tertbutyl ester hydrobromide

: 1191932-85-0
C₆₅H₁₁₂N₁₀O₁₆

Guidance literature:: 4,7-bis-tertbutoxycarbonylmethyl-1,4,7,10-tetraazacyclododec-1-yl acetic acid tertbutyl ester hydrobromide; With N,N,N',N'-tetramethylguanidine; In dichloromethane; for 2h;

C₁₃H₁₄Cl₂N₂O₄; With N-ethyl-N,N-diisopropylamine; In acetonitrile; for 24h; Inert atmosphere; Reflux;

Reference yield:

: 618-71-3
ethyl 3,5-dinitrobenzoate

: 1191932-85-0
C₆₅H₁₁₂N₁₀O₁₆

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride; hydrogen / palladium 10% on activated carbon / ethanol; water / 20 h / 6750.68 Torr / Buchi reactor

2.1: acetonitrile / Inert atmosphere

2.2: pH 7 / Inert atmosphere; Cooling with ice

3.1: N,N,N',N'-tetramethylguanidine / dichloromethane / 2 h

3.2: 24 h / Inert atmosphere; Reflux

With hydrogenchloride; hydrogen; N,N,N',N'-tetramethylguanidine; palladium 10% on activated carbon; In ethanol; dichloromethane; water; acetonitrile;

Reference yield:

: 1949-52-6
3,5-diamino-benzoic acid ethyl ester; hydrochloride

: 1191932-85-0
C₆₅H₁₁₂N₁₀O₁₆

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetonitrile / Inert atmosphere

1.2: pH 7 / Inert atmosphere; Cooling with ice

2.1: N,N,N',N'-tetramethylguanidine / dichloromethane / 2 h

2.2: 24 h / Inert atmosphere; Reflux

With N,N,N',N'-tetramethylguanidine; In dichloromethane; acetonitrile;