Technology Process of C14H11ClN6O
There total 4 articles about C14H11ClN6O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium 10% on activated carbon;
In
methanol;
for 20h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium dichromate; sulfuric acid / 5 h / 0 - 20 °C
2.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 4 h / 20 °C
2.2: 12 h / 20 °C
3.1: sodium azide; ammonium chloride / N,N-dimethyl-formamide / 24 h / 100 °C
4.1: hydrogen / palladium 10% on activated carbon / methanol / 20 h
With
sodium azide; sodium dichromate; oxalyl dichloride; sulfuric acid; hydrogen; ammonium chloride;
palladium 10% on activated carbon; N,N-dimethyl-formamide;
In
methanol; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 4 h / 20 °C
1.2: 12 h / 20 °C
2.1: sodium azide; ammonium chloride / N,N-dimethyl-formamide / 24 h / 100 °C
3.1: hydrogen / palladium 10% on activated carbon / methanol / 20 h
With
sodium azide; oxalyl dichloride; hydrogen; ammonium chloride;
palladium 10% on activated carbon; N,N-dimethyl-formamide;
In
methanol; dichloromethane; N,N-dimethyl-formamide;