C₃₇H₆₀N₂O₅Si₃

Base Information

Chemical Name:C₃₇H₆₀N₂O₅Si₃
CAS No.:1621925-46-9
Molecular Formula:C₃₇H₆₀N₂O₅Si₃
Molecular Weight:697.15
Hs Code.:

C<sub>37</sub>H<sub>60</sub>N<sub>2</sub>O<sub>5</sub>Si<sub>3</sub>

Synonyms:C₃₇H₆₀N₂O₅Si₃

Suppliers and Price of C₃₇H₆₀N₂O₅Si₃

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemicals and raw materials
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Total 2 raw suppliers

Chemical Property of C₃₇H₆₀N₂O₅Si₃

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of C₃₇H₆₀N₂O₅Si₃

There total 12 articles about C₃₇H₆₀N₂O₅Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 27607-77-8
trimethylsilyl trifluoromethanesulfonate

: C₃₁H₄₄N₂O₅Si

: 1621925-46-9
C₃₇H₆₀N₂O₅Si₃

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1002/chem.201400046

Reference yield:

: C₁₁H₁₄O₅

: 1621925-46-9
C₃₇H₆₀N₂O₅Si₃

Guidance literature:: Multi-step reaction with 11 steps

1.1: palladium 10% on activated carbon; hydrogen / methanol / 1 h / 760.05 Torr / Inert atmosphere

2.1: lithium hexamethyldisilazane / dichloromethane / 0.58 h / -78 - -50 °C / Inert atmosphere

2.2: 0.03 h / -50 °C / Inert atmosphere

3.1: dichloromethane / 20 °C / Inert atmosphere

4.1: palladium 10% on activated carbon; hydrogen / methanol / 1 h / 760.05 Torr / Inert atmosphere

5.1: sodium hydrogencarbonate / water; ethyl acetate / 20 °C

6.1: bis(cyclopentadienyl)titanium dichloride; zinc; cyclohexa-1,4-diene / tetrahydrofuran / 6 h / 0 °C / Inert atmosphere

7.1: triethylamine; dmap / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

8.1: triethylamine; dmap / dichloromethane / 2 h / 20 °C / Inert atmosphere

9.1: cyclohexa-1,4-diene; N-methylcarbazole / tetrahydrofuran; water / 12 h / Inert atmosphere; UV-irradiation

10.1: palladium 10% on activated carbon; hydrogen / methanol / 1 h / 760.05 Torr / Inert atmosphere

11.1: triethylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere

With dmap; bis(cyclopentadienyl)titanium dichloride; N-methylcarbazole; cyclohexa-1,4-diene; palladium 10% on activated carbon; hydrogen; sodium hydrogencarbonate; triethylamine; lithium hexamethyldisilazane; zinc; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate;
DOI:10.1002/chem.201400046

Reference yield:

: C₉H₁₀O₄

: 1621925-46-9
C₃₇H₆₀N₂O₅Si₃

Guidance literature:: Multi-step reaction with 10 steps

1.1: lithium hexamethyldisilazane / dichloromethane / 0.58 h / -78 - -50 °C / Inert atmosphere

1.2: 0.03 h / -50 °C / Inert atmosphere

2.1: dichloromethane / 20 °C / Inert atmosphere

3.1: palladium 10% on activated carbon; hydrogen / methanol / 1 h / 760.05 Torr / Inert atmosphere

4.1: sodium hydrogencarbonate / water; ethyl acetate / 20 °C

5.1: bis(cyclopentadienyl)titanium dichloride; zinc; cyclohexa-1,4-diene / tetrahydrofuran / 6 h / 0 °C / Inert atmosphere

6.1: triethylamine; dmap / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

7.1: triethylamine; dmap / dichloromethane / 2 h / 20 °C / Inert atmosphere

8.1: cyclohexa-1,4-diene; N-methylcarbazole / tetrahydrofuran; water / 12 h / Inert atmosphere; UV-irradiation

9.1: palladium 10% on activated carbon; hydrogen / methanol / 1 h / 760.05 Torr / Inert atmosphere

10.1: triethylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere

With dmap; bis(cyclopentadienyl)titanium dichloride; N-methylcarbazole; cyclohexa-1,4-diene; palladium 10% on activated carbon; hydrogen; sodium hydrogencarbonate; triethylamine; lithium hexamethyldisilazane; zinc; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate;
DOI:10.1002/chem.201400046