dibenzyl(imino)-λ⁶-sulfanone

Base Information

• Chemical Name: dibenzyl(imino)-λ⁶-sulfanone
• CAS No.: 67113-91-1
• Molecular Formula: C₁₄H₁₅NOS
• Molecular Weight: 245.345
• Mol file: 67113-91-1.mol

Synonyms:dibenzyl(imino)-λ⁶-sulfanone

Chemical Property of dibenzyl(imino)-λ⁶-sulfanone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of dibenzyl(imino)-λ⁶-sulfanone

There total 3 articles about dibenzyl(imino)-λ⁶-sulfanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

dibenzyl sulfide (538-74-9) → dibenzyl(imino)-λ6-sulfanone (67113-91-1)

Guidance literature:

With diacetoxyiodo-3,4,5-trifluorobenzene; water; ammonium carbonate; at 25 ℃; for 16h; Green chemistry;

DOI:10.1002/cssc.201903430

Reference yield: 86.0%

Dibenzyl sulfoxide (621-08-9) → dibenzyl(imino)-λ6-sulfanone (67113-91-1)

Guidance literature:

With [bis(acetoxy)iodo]benzene; ammonium carbamate; In methanol; at 25 ℃; for 0.5h;

DOI:10.1002/anie.201602320

Reference yield:

dimethyl sulfoxide (67-68-5,8070-53-9) → dibenzyl(imino)-λ6-sulfanone (67113-91-1)

Guidance literature:

Multistep reaction; (i) O-mesitylenesulfonyl hydroxylamine, (ii) Al₂O₃;

DOI:10.1248/cpb.27.2137

upstream raw materials:

Dibenzyl sulfoxide

dimethyl sulfoxide

dibenzyl sulfide

Downstream raw materials:

(Z)-N-(1,2-Dimethoxycarbonylvinyl)-dibenzylsulfoximin

(E)-N-(1,2-Dimethoxycarbonylvinyl)-dibenzylsulfoximin

S_.S-Dibenzyl-N-(p-tolylsulfonyl)-sulfoximin