14h-Anthra[2,1,9-mna]thioxanthen-14-one

Base Information

• Chemical Name: 14h-Anthra[2,1,9-mna]thioxanthen-14-one
• CAS No.: 16294-75-0
• Deprecated CAS: 54578-43-7
• Molecular Formula: C23H12OS
• Molecular Weight: 336.414
• Hs Code.: 2932999099
• European Community (EC) Number: 240-385-4
• DSSTox Substance ID: DTXSID0066032
• Nikkaji Number: J286.861J
• Wikidata: Q72508365
• Mol file: 16294-75-0.mol

Synonyms:14h-anthra[2,1,9-mna]thioxanthen-14-one;16294-75-0;Solvent Orange 63;C23H12OS;EINECS 240-385-4;14H-Anthra[219-mna]thioxanthen-14-one;14H-Anthra(2,1,9-mna)thioxanthen-14-one;EC 240-385-4;8-thiahexacyclo[10.10.2.02,7.09,23.013,18.020,24]tetracosa-1(23),2,4,6,9,11,13,15,17,20(24),21-undecaen-19-one;SCHEMBL374962;DTXSID0066032;C23-H12-O-S;MFCD00800439;AKOS015913744;4-Methyl-3-oxo-pentanoicacidethylester;anthra[2,1,9-mna]thioxanthen-14-one;AS-63962;CS-0155950;D70406;A882764;8-THIAHEXACYCLO[10.10.2.0(2),?.0?,(2)(3).0(1)(3),(1)?.0(2)?,(2)?]TETRACOSA-1(23),2(7),3,5,9,11,13(18),14,16,20(24),21-UNDECAEN-19-ONE

Chemical Property of 14h-Anthra[2,1,9-mna]thioxanthen-14-one

Chemical Property:

• Appearance/Colour: orange powder
• Vapor Pressure: 1.02E-14mmHg at 25°C
• Refractive Index: 1.815
• Boiling Point: 607.8 °C at 760 mmHg
• Flash Point: 382.7 °C
• PSA: 45.31000
• Density: 1.417 g/cm³
• LogP: 6.31210
• Storage Temp.: Sealed in dry,Room Temperature
• XLogP3: 6.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 0
• Exact Mass: 336.06088618
• Heavy Atom Count: 25
• Complexity: 558

Purity/Quality:

99% ^*data from raw suppliers

14H-Anthra[2,1,9-mna]thioxanthen-14-one 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C2C(=C1)C3=CC=C4C5=C(C=CC(=C35)C2=O)C6=CC=CC=C6S4

Technology Process of 14h-Anthra[2,1,9-mna]thioxanthen-14-one

There total 1 articles about 14h-Anthra[2,1,9-mna]thioxanthen-14-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C23H15NOS (41382-34-7) → 14H-anthra[2,1,9-m,n,a]thioxanthen-14-one (16294-75-0,54578-43-7)

Guidance literature:

With hydrogenchloride; sodium nitrite; In 1-methyl-pyrrolidin-2-one; water; at 50 - 70 ℃;

Reference yield: 67.0%

bromobenzene (108-86-1,52753-63-6) + 14H-anthra[2,1,9-m,n,a]thioxanthen-14-one (16294-75-0,54578-43-7) → 13-phenyl-14H-anthra[2,1,9-m,n,a]thioxanthen-14-one

Guidance literature:

bromobenzene; With magnesium; In tetrahydrofuran; at 59.84 ℃; for 0.5h;

14H-anthra[2,1,9-m,n,a]thioxanthen-14-one; In tetrahydrofuran; at 59.84 ℃;

DOI:10.1039/c9nj04851k

upstream raw materials:

C₂₃H₁₅NOS

Refernces

• 1、 -. "Benzothioxanthene dyes with improved application and toxicological properties". Page/Page column 8-9. . Retrieved 2009/08/16.