3-amino-N-methyl-4-[2-(trifluoromethyl)-1-pyrrolidinyl]benzenesuIfonamide

Base Information

Chemical Name:3-amino-N-methyl-4-[2-(trifluoromethyl)-1-pyrrolidinyl]benzenesuIfonamide
CAS No.:1316065-78-7
Molecular Formula:C₁₂H₁₆F₃N₃O₂S
Molecular Weight:323.339
Hs Code.:

Synonyms:3-amino-N-methyl-4-[2-(trifluoromethyl)-1-pyrrolidinyl]benzenesuIfonamide

Suppliers and Price of 3-amino-N-methyl-4-[2-(trifluoromethyl)-1-pyrrolidinyl]benzenesuIfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-amino-N-methyl-4-[2-(trifluoromethyl)-1-pyrrolidinyl]benzenesuIfonamide

Chemical Property:

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Technology Process of 3-amino-N-methyl-4-[2-(trifluoromethyl)-1-pyrrolidinyl]benzenesuIfonamide

There total 5 articles about 3-amino-N-methyl-4-[2-(trifluoromethyl)-1-pyrrolidinyl]benzenesuIfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1351094-58-0
N-methyl-3-nitro-4-[2-(trifluoromethyl)-1-pyrrolidinyl]benzenesulfonamide

: 1316065-78-7
3-amino-N-methyl-4-[2-(trifluoromethyl)-1-pyrrolidinyl]benzenesuIfonamide

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 0.75h; under 1810.07 Torr;

Reference yield:

: 1493-27-2,127723-77-7
ortho-nitrofluorobenzene

: 1316065-78-7
3-amino-N-methyl-4-[2-(trifluoromethyl)-1-pyrrolidinyl]benzenesuIfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: chlorosulfonic acid / 18 h / 100 °C

2: triethylamine / tetrahydrofuran / 1 h / -35 °C

3: 1,4-dioxane / 20 h / 110 °C / Sealed vessel

4: hydrogen / palladium on activated charcoal / ethanol / 0.75 h / 1810.07 Torr

With chlorosulfonic acid; hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; ethanol;

Reference yield:

: 6668-56-0
4-fluoro-3-nitrobenzene-1-sulfonyl chloride

: 1316065-78-7
3-amino-N-methyl-4-[2-(trifluoromethyl)-1-pyrrolidinyl]benzenesuIfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / tetrahydrofuran / 1 h / -35 °C

2: 1,4-dioxane / 20 h / 110 °C / Sealed vessel

3: hydrogen / palladium on activated charcoal / ethanol / 0.75 h / 1810.07 Torr

With hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; ethanol;