1-Benzylamino-2-phenyl-6,7-dihydro-3H,5H-benzochinolizin-3-on

Base Information

• Chemical Name: 1-Benzylamino-2-phenyl-6,7-dihydro-3H,5H-benzochinolizin-3-on
• CAS No.: 83609-78-3
• Molecular Formula: C₂₅H₂₂N₂O
• Molecular Weight: 366.462

Synonyms:1-Benzylamino-2-phenyl-6,7-dihydro-3H,5H-benzochinolizin-3-on

Chemical Property of 1-Benzylamino-2-phenyl-6,7-dihydro-3H,5H-benzochinolizin-3-on

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Technology Process of 1-Benzylamino-2-phenyl-6,7-dihydro-3H,5H-benzochinolizin-3-on

There total 1 articles about 1-Benzylamino-2-phenyl-6,7-dihydro-3H,5H-benzochinolizin-3-on which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

4-hydroxy-3-phenyl-1-azatricyclo[7.3.1.05,13]trideca-3,5,7,9(13)-tetraen-2-one (57625-49-7) + benzylamine (100-46-9) → 1-Benzylamino-2-phenyl-6,7-dihydro-3H,5H-benzochinolizin-3-on (83609-78-3)

Guidance literature:

for 24h; Heating;

DOI:10.1007/BF00809016

Reference yield: 81.0%

1-Benzylamino-2-phenyl-6,7-dihydro-3H,5H-benzochinolizin-3-on (83609-78-3) → 1-Amino-2-phenyl-6,7-dihydro-3H,5H-benzochinolizin-3-on (83609-69-2)

Guidance literature:

With hydrogen; palladium on activated charcoal; In acetic acid; for 2h; Heating;

DOI:10.1007/BF00809016

Reference yield: 17.0%

1-Benzylamino-2-phenyl-6,7-dihydro-3H,5H-benzochinolizin-3-on (83609-78-3) → 5-Phenyl-11,12-dihydro-10H,14H-benzoisochinolino<4,3-g>chinolizin-14-on (83609-74-9)

Guidance literature:

at 250 - 300 ℃; for 0.0833333h;

DOI:10.1007/BF00809016

upstream raw materials:

4-hydroxy-3-phenyl-1-azatricyclo[7.3.1.0^5,13]trideca-3,5,7,9⁽¹³⁾-tetraen-2-one

benzylamine

Downstream raw materials:

1-Amino-2-phenyl-6,7-dihydro-3H,5H-benzochinolizin-3-on

5-Phenyl-11,12-dihydro-10H,14H-benzoisochinolino<4,3-g>chinolizin-14-on

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