Welcome to LookChem.com Sign In|Join Free
  • or

Encyclopedia

Technology Process of C(CH3)3C6H4OC4H8OCH2C6H4N(C6H13)3(1+)*Br(1-)=C(CH3)3C6H4OC4H8OCH2C6H4N(C6H13)3Br

C(CH3)3C6H4OC4H8OCH2C6H4N(C6H13)3(1+)*Br(1-)=C(CH3)3C6H4OC4H8OCH2C6H4N(C6H13)3Br

Base Information
  • Chemical Name:C(CH3)3C6H4OC4H8OCH2C6H4N(C6H13)3(1+)*Br(1-)=C(CH3)3C6H4OC4H8OCH2C6H4N(C6H13)3Br
  • CAS No.:1237133-03-7
  • Molecular Formula:Br*C39H66NO2
  • Molecular Weight:660.863
  • Hs Code.:
C(CH<sub>3</sub>)3C<sub>6</sub>H<sub>4</sub>OC<sub>4</sub>H<sub>8</sub>OCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>N(C<sub>6</sub>H<sub>13</sub>)3<sup>(1+)</sup>*Br<sup>(1-)</sup>=C(CH<sub>3</sub>)3C<sub>6</sub>H<sub>4</sub>OC<sub>4</sub>H<sub>8</sub>OCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>N(C<sub>6</sub>H<sub>13</sub>)3Br

Synonyms:C(CH3)3C6H4OC4H8OCH2C6H4N(C6H13)3(1+)*Br(1-)=C(CH3)3C6H4OC4H8OCH2C6H4N(C6H13)3Br

Suppliers and Price of C(CH3)3C6H4OC4H8OCH2C6H4N(C6H13)3(1+)*Br(1-)=C(CH3)3C6H4OC4H8OCH2C6H4N(C6H13)3Br
Supply Marketing:
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
  • Manufacture/Brand
  • Chemicals and raw materials
  • Packaging
  • price
Total 0 raw suppliers
Chemical Property of C(CH3)3C6H4OC4H8OCH2C6H4N(C6H13)3(1+)*Br(1-)=C(CH3)3C6H4OC4H8OCH2C6H4N(C6H13)3Br
Chemical Property:
Purity/Quality:
Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
MSDS Files:
Useful:
Technology Process of C(CH3)3C6H4OC4H8OCH2C6H4N(C6H13)3(1+)*Br(1-)=C(CH3)3C6H4OC4H8OCH2C6H4N(C6H13)3Br

There total 5 articles about C(CH3)3C6H4OC4H8OCH2C6H4N(C6H13)3(1+)*Br(1-)=C(CH3)3C6H4OC4H8OCH2C6H4N(C6H13)3Br which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

tri-n-hexylamine
102-86-3

tri-n-hexylamine

C<sub>21</sub>H<sub>27</sub>BrO<sub>2</sub>
1237133-00-4

C21H27BrO2

C(CH<sub>3</sub>)3C<sub>6</sub>H<sub>4</sub>OC<sub>4</sub>H<sub>8</sub>OCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>N(C<sub>6</sub>H<sub>13</sub>)3<sup>(1+)</sup>*Br<sup>(1-)</sup>=C(CH<sub>3</sub>)3C<sub>6</sub>H<sub>4</sub>OC<sub>4</sub>H<sub>8</sub>OCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>N(C<sub>6</sub>H<sub>13</sub>)3Br
1237133-03-7

C(CH3)3C6H4OC4H8OCH2C6H4N(C6H13)3(1+)*Br(1-)=C(CH3)3C6H4OC4H8OCH2C6H4N(C6H13)3Br

Guidance literature:
In acetonitrile; at 80 ℃; for 16h;
DOI:10.1002/ejic.200901141

Reference yield:

[4-(4-chlorobutoxy)phenyl]methanol
1237132-94-3

[4-(4-chlorobutoxy)phenyl]methanol

C(CH<sub>3</sub>)3C<sub>6</sub>H<sub>4</sub>OC<sub>4</sub>H<sub>8</sub>OCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>N(C<sub>6</sub>H<sub>13</sub>)3<sup>(1+)</sup>*Br<sup>(1-)</sup>=C(CH<sub>3</sub>)3C<sub>6</sub>H<sub>4</sub>OC<sub>4</sub>H<sub>8</sub>OCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>N(C<sub>6</sub>H<sub>13</sub>)3Br
1237133-03-7

C(CH3)3C6H4OC4H8OCH2C6H4N(C6H13)3(1+)*Br(1-)=C(CH3)3C6H4OC4H8OCH2C6H4N(C6H13)3Br

Guidance literature:
Multi-step reaction with 4 steps
1: sodium iodide / butanone / 24 h / 80 °C
2: potassium carbonate / N,N-dimethyl-formamide / 48 h / 20 °C
3: phosphorus tribromide / toluene / 4 h / 0 - 20 °C
4: acetonitrile / 16 h / 80 °C
With phosphorus tribromide; potassium carbonate; sodium iodide; In N,N-dimethyl-formamide; toluene; acetonitrile; butanone;
DOI:10.1002/ejic.200901141

Reference yield:

C<sub>21</sub>H<sub>28</sub>O<sub>3</sub>
1237132-98-7

C21H28O3

C(CH<sub>3</sub>)3C<sub>6</sub>H<sub>4</sub>OC<sub>4</sub>H<sub>8</sub>OCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>N(C<sub>6</sub>H<sub>13</sub>)3<sup>(1+)</sup>*Br<sup>(1-)</sup>=C(CH<sub>3</sub>)3C<sub>6</sub>H<sub>4</sub>OC<sub>4</sub>H<sub>8</sub>OCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>N(C<sub>6</sub>H<sub>13</sub>)3Br
1237133-03-7

C(CH3)3C6H4OC4H8OCH2C6H4N(C6H13)3(1+)*Br(1-)=C(CH3)3C6H4OC4H8OCH2C6H4N(C6H13)3Br

Guidance literature:
Multi-step reaction with 2 steps
1: phosphorus tribromide / toluene / 4 h / 0 - 20 °C
2: acetonitrile / 16 h / 80 °C
With phosphorus tribromide; In toluene; acetonitrile;
DOI:10.1002/ejic.200901141
upstream raw materials:

C21H28O3

tri-n-hexylamine

C21H27BrO2

[4-(4-chlorobutoxy)phenyl]methanol

Post a RFQ

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

1 Customer Service

What can I do for you?
Get Best Price

Get Best Price for 1237133-03-7

Total 8 Pictures about this product