(Au(triphenylphosphine))2(naphthyl)

Base Information

Chemical Name:(Au(triphenylphosphine))2(naphthyl)
CAS No.:1189552-22-4
Molecular Formula:C₄₆H₃₆Au₂P₂
Molecular Weight:1044.67
Hs Code.:

Synonyms:(Au(triphenylphosphine))2(naphthyl)

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Chemical Property of (Au(triphenylphosphine))2(naphthyl)

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Technology Process of (Au(triphenylphosphine))2(naphthyl)

There total 1 articles about (Au(triphenylphosphine))2(naphthyl) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 4,4,5,5-tetramethyl-2-(2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)naphthalen-6-yl)-1,3,2-dioxaborolane

: 79384-10-4,14243-65-3
bromo(triphenylphosphine)gold(I)

: 1189552-22-4
(Au(triphenylphosphine))2(naphthyl)

Guidance literature:: With cesium carbonate; In isopropyl alcohol; benzene; suspending of Ph3PAuBr, C10H6(BO2C2Me4)2 and Cs2CO3 in isopropyl alcoholand charging into round-bottom flask; addn. of benzene; degassing, imme rsing in 40°C oil bath and stirring under Ar for 24 h; removal solvent by rotary evapn.; extn. into CH2Cl2; filtration, removalCH2Cl2 by evapn., trituration with pentane; vac. filtration; trituratin g with hexanes; dissolving in CH2Cl2; filtration, layering ether onto CH2Cl2 soln., crystn., elem. anal.;
DOI:10.1021/om9005214