3,5-bis(4-(4-hydroxyphenyl)phenyl)benzyl alcohol

Base Information

Chemical Name:3,5-bis(4-(4-hydroxyphenyl)phenyl)benzyl alcohol
CAS No.:429696-96-8
Molecular Formula:C₃₁H₂₄O₃
Molecular Weight:444.53
Hs Code.:

Synonyms:3,5-bis(4-(4-hydroxyphenyl)phenyl)benzyl alcohol

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Chemical Property of 3,5-bis(4-(4-hydroxyphenyl)phenyl)benzyl alcohol

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Technology Process of 3,5-bis(4-(4-hydroxyphenyl)phenyl)benzyl alcohol

There total 5 articles about 3,5-bis(4-(4-hydroxyphenyl)phenyl)benzyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 429696-94-6
methyl 3,5-bis(4-(4-hydroxyphenyl)phenyl)benzoate

: 429696-96-8
3,5-bis(4-(4-hydroxyphenyl)phenyl)benzyl alcohol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 3h; Heating;
DOI:10.1016/S0040-4020(01)01113-9

Reference yield:

: 51329-15-8
methyl 3,5-dibromobenzoate

: 429696-96-8
3,5-bis(4-(4-hydroxyphenyl)phenyl)benzyl alcohol

Guidance literature:: Multi-step reaction with 3 steps

1.1: Mg; 1,2-dibromoethane / tetrahydrofuran / Heating

1.2: trimethyl borate / tetrahydrofuran / 0.33 h / Heating

1.3: 11.1 g / Na₂CO₃ / Pd(PPh₃)4 / toluene; H₂O; ethanol / 48 h / Heating

2.1: 94 percent / conc. HCl / CHCl₃; propan-2-ol / Heating

3.1: 95 percent / LiAlH₄ / tetrahydrofuran / 3 h / Heating

With hydrogenchloride; lithium aluminium tetrahydride; magnesium; ethylene dibromide; In tetrahydrofuran; chloroform; isopropyl alcohol; 1.3: Suzuki coupling reaction;
DOI:10.1016/S0040-4020(01)01113-9

Reference yield:

: 29558-77-8
4-bromo-4'-hydroxybiphenyl

: 429696-96-8
3,5-bis(4-(4-hydroxyphenyl)phenyl)benzyl alcohol

Guidance literature:: Multi-step reaction with 4 steps

1.1: NaH / tetrahydrofuran / 1 h / 20 °C

1.2: tetrahydrofuran / 20 °C

2.1: Mg; 1,2-dibromoethane / tetrahydrofuran / Heating

2.2: trimethyl borate / tetrahydrofuran / 0.33 h / Heating

2.3: 11.1 g / Na₂CO₃ / Pd(PPh₃)4 / toluene; H₂O; ethanol / 48 h / Heating

3.1: 94 percent / conc. HCl / CHCl₃; propan-2-ol / Heating

4.1: 95 percent / LiAlH₄ / tetrahydrofuran / 3 h / Heating

With hydrogenchloride; lithium aluminium tetrahydride; sodium hydride; magnesium; ethylene dibromide; In tetrahydrofuran; chloroform; isopropyl alcohol; 2.3: Suzuki coupling reaction;
DOI:10.1016/S0040-4020(01)01113-9