methyl 5,6-dihydro-2-methoxy-4-benzyl-imidazo<1,2-b><1,2,4> triazole-5-carboxylate

Base Information

Chemical Name:methyl 5,6-dihydro-2-methoxy-4-benzyl-imidazo<1,2-b><1,2,4> triazole-5-carboxylate
CAS No.:139924-79-1
Molecular Formula:C₁₄H₁₆N₄O₃
Molecular Weight:288.306
Hs Code.:

Synonyms:methyl 5,6-dihydro-2-methoxy-4-benzyl-imidazo<1,2-b><1,2,4> triazole-5-carboxylate

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Chemical Property of methyl 5,6-dihydro-2-methoxy-4-benzyl-imidazo<1,2-b><1,2,4> triazole-5-carboxylate

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Technology Process of methyl 5,6-dihydro-2-methoxy-4-benzyl-imidazo<1,2-b><1,2,4> triazole-5-carboxylate

There total 2 articles about methyl 5,6-dihydro-2-methoxy-4-benzyl-imidazo<1,2-b><1,2,4> triazole-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 2.3%

: 21384-53-2,31907-91-2,196965-62-5
methyl 1-benzylaziridine-2-carboxylate

: 15777-61-4
3-bromo-5-methoxy-1H-1,2,4-triazole

: methyl 2-benzylamino-3-(3-methoxy-5-bromo-1,2,4-triazol-1-yl)-propionate

: 139924-79-1
methyl 5,6-dihydro-2-methoxy-4-benzyl-imidazo<1,2-b><1,2,4> triazole-5-carboxylate

: 139924-78-0
methyl 2-benzylamino-3-(3-bromo-5-methoxy-1,2,4-triazol-1-yl)-propionate

Guidance literature:: With boron trifluoride diethyl etherate; In tetrahydrofuran; at 60 ℃; for 3h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1016/S0957-4166(00)82312-5

Reference yield:

: 21384-53-2,31907-91-2,196965-62-5
methyl 1-benzylaziridine-2-carboxylate

: 15777-61-4
3-bromo-5-methoxy-1H-1,2,4-triazole

: 139924-79-1
methyl 5,6-dihydro-2-methoxy-4-benzyl-imidazo<1,2-b><1,2,4> triazole-5-carboxylate

Guidance literature:: With hydrogenchloride; boron trifluoride diethyl etherate; Yield given. Multistep reaction; 1.) THF, 60 deg C, 3 h, 2.) MeOH, reflux, 8 h;
DOI:10.1016/S0957-4166(00)82312-5